Archive for November, 2013

HOT Articles in Analytical Methods

Take a look at our new HOT articles just published in Analytical Methods! These papers are all free to read for the next three weeks. Enjoy!

Development of a rapid detection method for seven pesticides in cucumber using hollow fibre liquid phase microextraction and ion mobility spectrometry
Jianfeng Wang, Zhongxia Zhang, Zhenxia Du and Wenjun Sun
Anal. Methods, 2013, 5, 6592-6597
DOI: 10.1039/C3AY40667A, Paper

Molecularly imprinted polymer-liquid chromatography/fluorescence for the selective clean-up of hydroxylated polycyclic aromatic hydrocarbons in soils
Oriol Baltrons, Montserrat López-Mesas, Cristina Palet, Franck Le Derf and Florence Portet-Koltalo
Anal. Methods, 2013, 5, 6297-6305
DOI: 10.1039/C3AY41227J, Paper

Analysis of cadmium-based pigments with time-resolved photoluminescence
Anna Cesaratto, Cosimo D’Andrea, Austin Nevin, Gianluca Valentini, Francesco Tassone, Roberto Alberti, Tommaso Frizzi and Daniela Comelli
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41585F, Paper

Facile detection of latent fingerprints on various substrates based on perylene probe excimer emission
Fangyuan Wang, Jian Chen, Huipeng Zhou, Wenying Li, Qingfeng Zhang and Cong Yu
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41802B, Communication

Investigation into dissolved neutral sugars and their microbial conversion in natural and artificially produced dissolved organic matter using ion chromatography with pulsed amperometric detection and reversed-phase liquid chromatography-high resolution mass spectrometry
Sara Sandron, Richard Wilson, Ruth Larragy, Margaret V. McCaul, Pavel N. Nesterenko, Brian Kelleher and Brett Paull
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41549J, Paper

Simple density-based particle separation in a microfluidic chip
Daisuke Sugiyama, Yuki Teshima, Kenichi Yamanaka, Maria Portia Briones-Nagata, Masatoshi Maeki, Kenichi Yamashita, Masashi Takahashi and Masaya Miyazaki
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY40971F, Technical Note

Hydrophilic interaction/cation-exchange chromatography for glycopeptide enrichment by using a modified strong-cation exchange material
Linlin Chen, Xuefang Dong, Liwei Cao, Zhimou Guo, Long Yu, Lijuan Zou and Xinmiao Liang
Anal. Methods, 2013, 5, 6919-6924
DOI: 10.1039/C3AY41590B, Paper

A luminescence-based assay of UDP-sugar producing pyrophosphorylases
Daniel Decker, Stina Lindberg, Jonas Eriksson and Leszek A. Kleczkowski
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41811A, Communication

A nuclear forensic method for determining the age of radioactive cobalt sources
Luc Charbonneau, Jean-Michel Benoit, Slobodan Jovanovic, Nadereh St-Amant, Stephen Kiser, Michael W. Cooke, Jean-François Mercier, Kathy Nielsen, David Kelly, Pavel Samuleev, Raphael Galea, Kimberly Moore, Patrick R. B. Saull, David B. Chamberlain, Jennifer L. Steeb, Donald G. Graczyk, Yifen Tsai, Vivian S. Sullivan, Ike C. Dimayuga, Youqing Shi, Raghu Rao and Dominic Larivière
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41443D, Paper

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Answers to Endangered Animals Lies in their Scat

LC-MS for Animal Identification

LC-MS for Animal Identification

Studying rare or endangered species of wild animals is no easy task. Analysis of animal tracks and fecal matter left behind can provide some clues for species identification, as well as insight into animal behavior and habitation. However, these identification signs are elusive, and often confounded by variations in environmental conditions, as well as animal health and diet. While methods of molecular analysis such as DNA sequence analysis of animal scat samples can provide more informative answers, DNA contamination from other mammals can make accurate identification difficult. To circumvent some of these limitations, Udaya Nasini, Ali Shaikh and colleagues from the University of Arkansas in Little Rock, USA, have demonstrated the use of liquid chromatography-mass spectrometry (LC-MS) to determine the composition of bile acids in scat samples. Analysis using LC-MS provides a metabolic pattern that is characteristic of a distinct species, and in turn enables effective identification.

Read more about this work by accessing the link below. This paper will be free to read for the next three weeks.

Let us know what your thoughts are by leaving a comment below!

Determination of bile acid profiles in scat samples of wild animals by liquid chromatography-electrospray mass spectrometry
Udaya B. Nasini, Nandan Peddi, Punnamchandar Ramidi, Yashraj Gartia, Anindya Ghosh and Ali U. Shaikh
Anal. Methods, 2013,5, 6319-6324
DOI: 10.1039/C3AY41048J

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Detecting iron the smart way

Spanish scientists have developed a way to quantitatively measure the amount of iron in a solution using a colour changing material and photos taken on a smartphone. Detecting iron the smart way

Iron is present in almost every aspect of our lives but an excess, known as iron overload, can cause significant long term effects ranging from liver damage to arthritis as a result of iron deposition in organs or joints. As such, the amount of iron in a variety of environments needs to be carefully monitored.

Unlike traditional quantitative techniques, which require removing samples to the lab for assessment by trained specialists, the new approach devised by José Miguel García and colleagues at the University of Burgos can return a result within 15 minutes. Central to the technique is 8-hydroxyquinoline, a particularly stable iron chelator, which is immobilised on a polymer disk and will change colour depending on the amount of iron chelated to it.

To read the full article, please visit Chemistry World.

Solid sensory polymer substrates for the quantification of iron in blood, wine and water by a scalable RGB technique
Saúl Vallejos, Asunción Muñoz, Saturnino Ibeas, Felipe Serna, Félix Clemente García and José Miguel García
J. Mater. Chem. A, 2013, Advance Article
DOI: 10.1039/C3TA12703F

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HOT Articles in Analytical Methods

Take a look at our new HOT articles just published in Analytical Methods! These papers are all free to read for the next three weeks. Enjoy!

Combination of effective machine learning techniques and chemometric analysis for evaluation of Bupleuri Radix through high-performance thin-layer chromatography
Xiaoping Cheng, Hongmin Cai, Ping He, Yue Zhang and Runtiao Tian
Anal. Methods, 2013,5, 6325-6330
DOI: 10.1039/C3AY41132J, Paper

Direct molecular detection of SRY gene from unamplified genomic DNA by metal-enhanced fluorescence and FRET
Danny Brouard, Olivier Ratelle, A. Guillermo Bracamonte, Maryse St-Louis and Denis Boudreau
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C3AY41428K, Communication

Towards an uncertainty paradigm of detection capability
Michael Thompson and Stephen L. R. Ellison
Anal. Methods, 2013,5, 5857-5861
DOI: 10.1039/C3AY41209A, Editorial

Fluorescence imaging for biofoulants detection and monitoring of biofouled strength in reverse osmosis membrane
Jinhee Choi, Wooyeol Choi, Hyunjung Kim, Aamir Alaud-din, Kyung Hwa Cho, Joon Ha Kim, Hyuk Lim, Robert W. Lovitt and In Seop Chang
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C3AY40870A, Paper

A highly selective and sensitive fluorescence ratiometric probe for cyanide and its application for the detection of cyanide in natural water and biological samples
Lingliang Long, Liping Zhou, Lin Wang, Suci Meng, Aihua Gong, Fengyi Du and Chi Zhang
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C3AY41475B, Paper

Planar microfluidic devices in flow modulated comprehensive two dimensional gas chromatography for challenging petrochemical applications
Robert A. Shellie, Hernan J. Cortes, Ronda Gras and Jim Luong
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C3AY41198B, Paper

A general method for optimizing the parameter of α/β discrimination in liquid scintillation counting
Xiao-gui Feng, Qian-ge He, Jian-chen Wang and Jing Chen
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C3AY41534A, Paper

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Top ten most accessed Analytical Methods articles for July-September 2013

Here are the top ten most accessed Analytical Methods articles from July to September 2013.

Photocatalytic reduction of CO2: a brief review on product analysis and systematic methods
Jindui Hong, Wei Zhang, Jia Ren and Rong Xu  
Anal. Methods, 2013,5, 1086-1097
DOI: 10.1039/c2ay26270c

Let there be chip—towards rapid prototyping of microfluidic devices: one-step manufacturing processes
Ansgar Waldbaur, Holger Rapp, Kerstin Länge and Bastian E. Rapp  
Anal. Methods, 2011,3, 2681-2716
DOI: 10.1039/c1ay05253e

‘It’s not easy being green’: a spectroscopic study of green pigments used in illuminated manuscripts
Paola Ricciardi, Anuradha Pallipurath and Kristine Rose  
Anal. Methods, 2013,5, 3819-3824
DOI: 10.1039/c3ay40530c

Microscale separation of immiscible liquids using a porous capillary
James H. Bannock, Thomas W. Phillips, Adrian M. Nightingale and John C. deMello  
Anal. Methods, 2013,5, 4991-4998
DOI: 10.1039/c3ay41251b

Magnetic (nano)materials as an useful tool for sample preparation in analytical methods. A review
Angel Ríos, Mohammed Zougagh and Mohamed Bouri
Anal. Methods, 2013,5, 4558-4573
DOI: 10.1039/c3ay40306h

The evolution of chemometrics
Richard G. Brereton  
Anal. Methods, 2013,5, 3785-3789
DOI: 10.1039/c3ay90051g

Detection of apoptosis: A review of conventional and novel techniques
Michelle M. Martinez, Randall D. Reif and Dimitri Pappas  
Anal. Methods, 2010,2, 996-1004
DOI: 10.1039/c0ay00247j

Rhodamine and BODIPY chemodosimeters and chemosensors for the detection of Hg2+, based on fluorescence enhancement effects
M. J. Culzoni, A. Muñoz de la Peña, A. Machuca, H. C. Goicoechea and R. Babiano  
Anal. Methods, 2013,5, 30-49
DOI: 10.1039/c2ay25769f

Application of Raman spectroscopy for the differentiation of lipstick traces
Fatma Salahioglu, Michael J. Went and Stuart J. Gibson  
Anal. Methods, 2013,5, 5392-5401
DOI: 10.1039/c3ay41274a

Electrochemical impedance spectroscopy: an overview of bioanalytical applications
Edward P. Randviir and Craig E. Banks
Anal. Methods, 2013,5, 1098-1115
DOI: 10.1039/c3ay26476a

If you have any comments or thoughts on any of these articles, we welcome you to write these in the comment box below.

Do you fancy submitting an article to Analytical Methods? Why not submit to us here today or alternatively email us with your suggestions!

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