Archive for November, 2012

Fingerprints on demand

An on-demand system to print artificial fingerprints has been developed by US scientists. The fingerprints could be used to ensure that detection equipment for explosives and narcotics, such as those used in airports and federal prisons, are working as expected.

Jessica Staymates and her team at the National Institute of Standards and Technology, Gaithersburg, incorporated the oily substance found in fingerprints – sebum – into explosive test materials to provide a realistic challenge for trace detection technologies. ‘When someone handles explosive or narcotics materials, they inevitably contaminate themselves, their clothing and belongings with micrometre-sized particles of the material,’ explains Staymates. ‘It is generally believed that these trace residues are commonly spread via fingerprints.’

White light (left) and polarised light micrographs of sebum-heptane-RDX-polyisobutylene mix printed in a fingerprint-like array

White light (left) and polarised light micrographs of sebum-heptane-RDX-polyisobutylene mix printed in a fingerprint-like array

 To read the full article please visit Chemistry World.

Evaluation of a drop-on-demand micro-dispensing system for development of artificial fingerprints
Jessica L. Staymates, Matthew E. Staymates and Greg Gillen
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY26167G

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)

Identifying Toxic Chemicals in Fish Poisoning

Jiang et al., Anal. Methods, 2013, Advance Article

Jiang et al., Anal. Methods, 2013, Advance Article

In regions where commercial fisheries play a major role in the economy, large scale poisoning of the aquaculture can have a devastating effect. It is important for forensic investigations that the toxic chemicals can be identified and quantitated accurately. Haipeng Jiang and Jing Zou at the Wuhan Institute of Technology have developed an LC-MS/MS method for the simultaneous determination of three commonly used fishpond poisons: pentachlorophenol, niclosamide and fenpropathrin. These compounds are particularly challenging to detect by conventional GC-MS methods. The authors tested their procedure using a real life case study of fish poisoning in Hubei Province, China, where an unknown toxin diminished the production of farmed pearls in the area in 2010.

This paper will be free to read until Dec 10th.

Simultaneous determination of pentachlorophenol, niclosamide and fenpropathrin in fishpond water using an LC-MS/MS method for forensic investigation
Haipeng Jiang,  Yinhua Zhang,  Xiangguo Chen,  Jizhong Lv and Jing Zou
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY25685A

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)

Analytical Methods Issue 12 now online

Simple, rapid and label-free colorimetric assay for arsenic based on unmodified gold nanoparticles and a phytochelatin-like peptide

Liu et al., Anal. Methods, 2012, 4, 3937

For this last issue of 2012 we have three lovely covers for you to enjoy. The water-themed front cover comes from Lin Liu at Anyang Normal University, who together with a team from China has developed a colorimetric assay for the determination of arsenic. This was applied to the testing of drinking water and could detect levels set by the World Health Organization.

Simple, rapid and label-free colorimetric assay for arsenic based on unmodified gold nanoparticles and a phytochelatin-like peptide
Ning Xia, Yunfeng Shi, Renchun Zhang, Feng Zhao, Feng Liu and Lin Liu
Anal. Methods, 2012, 4, 3937-3941
DOI: 10.1039/C2AY25803J

Determination of carbonate ion contents in layered double hydroxides by FTIR spectrometry

Miyake et al., Anal. Methods, 2012, 4, 3925

Our inside front cover comes from Okayama University, Japan, where a team led by Michihiro Miyake has been looking at layered double hydroxides, often used as inorganic hosts for developing functional materials.

Determination of carbonate ion contents in layered double hydroxides by FTIR spectrometry
Toshiyuki Tanaka, Yoshikazu Kameshima, Shunsuke Nishimoto and Michihiro Miyake
Anal. Methods, 2012, 4, 3925-3927
DOI: 10.1039/C2AY25850A

Directional surface plasmon-coupled emission of CdTe quantum dots and its application in Hg(II) sensing

Li et al., Anal. Methods, 2012, 4, 3956

The striking image on the back cover showcases research into surface plasmon-coupled emission-based sensors by Professor Yao-Qun Li’s research group from the Department of Chemistry and Key Laboratory of Analytical Sciences, Xiamen University, Xiamen, China.

Directional surface plasmon-coupled emission of CdTe quantum dots and its application in Hg(II) sensing
Xiao-Qing Liu, Qian Liu, Shuo-Hui Cao, Wei-Peng Cai, Yu-Hua Weng, Kai-Xin Xie and Yao-Qun Li
Anal. Methods, 2012, 4, 3956-3960
DOI: 10.1039/C2AY25541C

These three cover papers will be free to read for 6 weeks.

Preparation of aligned porous silica monolithic capillary columns and their evaluation for HPLC

Zhang et al., Anal. Methods, 2012, 4, 3942

This issue also features a HOT article by Haifei Zhang and colleagues at the Univeristy of Liverpool. Capillary columns were prepared and evaluated on their use in HPLC. This paper will be free for 2 weeks.

Preparation of aligned porous silica monolithic capillary columns and their evaluation for HPLC
Adham Ahmed, Peter Myers and Haifei Zhang
Anal. Methods, 2012, 4, 3942-3947
DOI: 10.1039/C2AY25671A

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)

The importance of water quality in the laboratory

4 December 2012, 13:00 – 14:00 (GMT)

Free webinar

Speaker: Dr Estelle Riché – Senior Scientist, Merck Millipore

How are water contaminants affecting your lab results?

Join us for our next live and interactive Chemistry World webinar to learn why and how water is purified to yield the various water qualities used in the laboratory.

By the end of this free one-hour knowledge-share, you will be able to:

  • identify the different contaminants potentially present in laboratory water
  • understand the potential impact of these contaminants on laboratory applications such as HPLC, LC-MS, etc.
  • understand how various water purification technologies remove these contaminants from laboratory water
  • make better choices for the water you use in your laboratory work

Click here to find out more and register for free 

This webinar is brought to you by Chemistry World in partnership with Merck Millipore.

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)

HOT articles in Analytical Methods

Take a look below at some wonderful HOT articles we’ve recently published this month in Analytical Methods. There are papers covering a variety of fields, including fluorimetry, catalytic cracking, live cell staining and supramolecular chemistry. These HOT papers will be free to read until Dec 5th.

Study on the supramolecular interaction of astemizole with cucurbit[7]uril and its analytical application
Guang-Quan Wang ,  Li-Ming Du ,  Yu-Hua Guo ,  Yan-Fang Qin ,  Jun-Wen Wang and Hao Wu
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY25929J 
 
Xanthone based Pb2+ selective turn on fluorescent probe for living cell staining
Debasis Karak ,  Arnab Banerjee ,  Sisir Lohar ,  Animesh Sahana ,  Subhra Kanti Mukhopadhyay ,  Sushanta. S. Adhikari and Debasis Das
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY25935D 
 

Direct determination of nickel in xylene solutions of raw material for catalytic cracking with application of graphite furnace atomic absorption spectrometry
Zofia Kowalewska
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY25920F 
 
Resonant waveguide grating (RWG): overcoming the problem of angular sensitivity by conical, broad-band illumination for fluorescence measurements
Tarmo Nuutinen ,  Petri Karvinen ,  Jussi Rahomäki and Pasi Vahimaa
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY25470K

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)

A Novel Assay for Studying DNA Repair

A novel DNAzyme-based colorimetric assay for the detection of hOGG1 activity with lambda exonuclease cleavage

Yu et al., Anal. Methods, 2013, Advance Article

Mutation, apoptosis and cancer can develop from damaged DNA, however the cell produces proteins capable of repairing DNA to prevent these dangerous effects. One of these proteins produced by cells, 8-oxoG DNA glycosylase/AP lyase (hOGG1), targets DNA lesions caused by reactive oxygen species. Typically studying this glycosylase requires large instrumentation, such as HPLC, or radioactive labeling. Ru-Qin Yu and coworkers at Hunan University developed a system, where the hOGG1 cleaves at the mismatch site on a DNA strand, and releases a DNAzyme mimetic, which produces a colored signal. This rapid and sensitive colorimetric assay measured the activity of hOGG1 for a range of concentrations, with an affordable DNA probe, and user-friendly instrumentation.

This paper will be free to read until Nov 30th.

A novel DNAzyme-based colorimetric assay for the detection of hOGG1 activity with lambda exonuclease cleavage
Shu-Cheng Liu, Hui-Wang Wu, Jian-hui Jiang, Guo-Li Shen and Ru-Qin Yu
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY26018B

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)

HOT articles in Analytical Methods this October

Analytical Methods, Oustide front cover, Issue 10, 2012Take a look below at some wonderful HOT articles we’ve recently published this month in Analytical Methods. There are papers covering a large variety of fields, including the analysis of cosmetics, semivolatiles in drinking water, microarrays, and refrigerant systems. These HOT papers will be free to read until November 19th.

Preparation of aligned porous silica monolithic capillary columns and their evaluation for HPLC
Adham Ahmed, Peter Myers and Haifei Zhang
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25671A

Fabricating three-dimensional hydrogel oligonucleotide microarrays to detect single nucleotide polymorphisms
Xia Liu, Tao Li, Dianjun Liu and Zhenxin Wang
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25904D

Measurement of iodide and caffeine content in cellulite reduction cosmetic products sold in the European market
Emilia Marchei, Daniela De Orsi, Carmine Guarino, Stefano Dorato, Roberta Pacifici and Simona Pichini
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25761K

A novel outlook on detecting microbial contamination in cosmetic products: analysis of biomarker volatile compounds by solid-phase microextraction gas chromatography-mass spectrometry
Gerardo Alvarez-Rivera, Trinidad De Miguel, Maria Llompart, Carmen Garcia-Jares, Tomas Gonzalez Villa and Marta Lores
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25833A

Analytical Methods, Inside front cover, Issue 10, 2012Development of EPA Method 525.3 for the analysis of semivolatiles in drinking water
Paul E. Grimmett and Jean W. Munch
Anal. Methods, 2013, Advance Article
DOI: 10.1039/C2AY25880C

Determination of the Raman depolarization ratio in optically active samples
Johannes Kiefer and Malte Kaspereit
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25987G

A compact comprehensive two-dimensional gas chromatography (GC×GC) approach for the analysis of biogenic VOCs
Samuel J. Edwards, Alastair C. Lewis, Stephen J. Andrews, Richard T. Lidster, Jacqueline F. Hamilton and Christopher N. Rhodes
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25710F

A sensor probe for the continuous in situ monitoring of ammonia leakage in secondary refrigerant systems
Raman Subramanian, Karl Crowley, Aoife Morrin and Anthony J. Killard
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25688F

Digg This
Reddit This
Stumble Now!
Share on Facebook
Bookmark this on Delicious
Share on LinkedIn
Bookmark this on Technorati
Post on Twitter
Google Buzz (aka. Google Reader)