Archive for May, 2015

Getting closer to secrets on the seabed

Graphical Abstract

Researchers from Spain have engineered a laser spectrometer to analyse solids underwater that they hope to eventually develop for deep sea research.1

Stand-off laser induced breakdown spectroscopy (ST-LIBS) is a technique to identify the elemental composition of solids at a distance, enabling safe analysis of explosive, radioactive or toxic compounds.2 While this technique is well-developed and widely used in air – Javier Laserna and coworkers at the University of Malaga built a ST-LIBS system able to differentiate between common explosives and contaminants such as hand cream or motor oil3 – there is no current technology to apply it underwater.

Read the full article over at Chemistry World >>


A study of underwater stand-off laser-induced breakdown spectroscopy for chemical analysis of objects in the deep ocean
F. J. Fortes, S. Guirado, A. Metzinger and J. J. Laserna
J. Anal. At. Spectrom., 2015, 30, 1050-1056
DOI: 10.1039/C4JA00489B, Paper

Do you fancy submitting an article to JAAS? Why not submit to us here today or alternatively email us with your suggestions!

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JAAS Emerging Investigator Lectureship awardees

We are delighted to announce the winners of the inaugural JAAS Emerging Investigator Lectureship. Launched to coincide with the 30th anniversary of the journal, the lectureship will be awarded annually from 2015 to recognise and support an emerging scientist working in the area of atomic spectrometry in the early stages of their independent career.

With so many exceptional and highly deserving nominations, it was decided to award the JAAS Emerging Investigator Lectureship to two winners this year.

Congralutaions to Gerardo Gamez (Texas Tech University) and Lara Lobo Revilla (University of Oviedo)!

Introducing Lara Lobo Revilla:

Lara Lobo Revilla

Lara Lobo Revilla

Lara Lobo Revilla is a “Marie Curie Clarin-Cofund” postdoctoral researcher at the University of Oviedo since October 2014. She studied Chemistry at the University of Oviedo, where she also started her PhD in 2006 working on a European project aimed at the instrumental development and analytical applications of a prototype based on Glow Discharge-Time of Flight Mass Spectrometry. Under the supervision of Prof. Rosario Pereiro and Dr. Nerea Bordel, she obtained her PhD degree in 2011 and was given the Extraordinary Doctorate Award (Physical and Analytical Chemistry). After she finished her PhD she got an IEF Marie-Curie Fellowship and joined the A&MS group of Prof. Frank Vanhaecke in the Analytical Chemistry Department at Ghent University (Belgium). Her research for about 3 years at UGent has mainly dealt with isotopic analysis for provenancing ancient glass. Currently, she is involved in the development of analytical methods to obtain elemental, molecular and isotopic information based on the use of different analytical mass spectrometry techniques.

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Introducing Gerardo Gamez:

Gerardo Gamez

Gerardo Gamez obtained his B.Sc., summa cum laude, and M.S. in Chemistry at the University of Texas at El Paso where he performed research with Prof. Gardea-Torresdey in environmental chemistry. He obtained his PhD in Analytical Chemistry at Indiana University-Bloomington with Prof. Hieftje where he performed research in plasma-based analytical spectrochemistry. During this time he obtained fellowships from the ACS-DAC and MERC, as well as the first Richard Payling Award. His postdoctoral work at ETH Zurich with Prof. Zenobi was in the area of ambient molecular MS. He then worked as a Scientist at EMPA Thun in the field of materials characterization by atomic spectroscopy. In the fall of 2013 he joined the faculty of the Department of Chemistry and Biochemistry at Texas Tech University. His research group focuses on instrumentation and method development of high-throughput chemical imaging techniques via GDOES elemental mapping, ambient desorption/ionization MS sources, as well as performing fundamental studies to better understand laboratory plasmas. He has more than 50 peer-reviewed publications (h-index 24), and given more than 30 oral presentations (including 15 invited lectures). He has also served as president of the Indiana Section of the Society for Applied Spectroscopy, coordinator of an EC Marie Curie Research Training Network (GLADNET, 16 partners, 11 countries), co-organizer of the 1st International Symposium on Glow Discharge Spectroscopy, and chair of the Atomic Spectroscopy section of the SCIX conference.

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The Next Generation- An Interview with Flávio V. Nakadi

Today we interview a truly exceptional young PhD student, a true expert in various ancient arts (e.g., origami and brewing beer), Flávio Venâncio Nakadi, a PhD student at the Universidade de São Paulo, working under the supervision of Prof. Dr. Márcia A.M.S. da Veiga.


Flávio in his lab in Ribeirão Preto, Brazil

Q: Who or what inspired you to become a scientist?

A: I believe the first time I said “I want to be a scientist” I was 7 years old. I was always curious about how everything works: from nature to technology. I used to watch a TV show called “Beakman’s World”, which showed many chemical and physical phenomena and explained them in an easy way that a child could “comprehend”. It fascinated me! Later, my mother gave me a chemistry kit when I was 10 years old, which was the first step into my career.

During Analytical Chemistry classes, after my first contact with equipment, in particular spectrometers, I knew that I would study in this area. I had the opportunity to begin my master’s degree with my supervisor, Prof. Dr. da Veiga with atomic absorption spectrometry and, since 2009, I am working in AAS.

Q: Why did you choose your research group/University and what factors influenced your choice?

A: The University of São Paulo is one of the best Universities in Latin America; therefore, the choice was natural. However, I chose it because it is located in the city where I live. When I started my studies in Chemistry, I knew I made the right choice. Before working with atomic spectrometry, I tried electrochemistry and inorganic chemistry. Both areas were great, but they were not exactly what I was looking for. I realized what I wanted to do during analytical chemistry classes: to work with analytical instruments. Prof. Dr. da Veiga was new in our department and the only researcher who worked with elemental analysis (AAS). I could work with her and see her laboratory and research group grow, and I am very grateful that I could share this experience with all of them.

Q: Can you explain a bit the purpose of your current research activities?

A: High-resolution continuum source molecular absorption spectrometry (HR CS MAS) is a technique that still shows new possibilities for elemental analysis. The determination of non-metals by monitoring the absorbance of diatomic molecules with an AAS instrument has brought new possibilities to the field. I have studied mainly the determination of sulfur via CS molecule in coal and diesel samples, the latter as direct analysis with Pd nanoparticles as chemical modifier.

Furrthermore, a new methodology that I have developed in the lab of Prof. Dr. Resano has enabled isotopic analysis with HR CS MAS. There is always a wavelength shift between the atomic lines of different isotopes, but it is generally too small for detection (less than 1 pm). However, diatomic molecules show larger isotopic shifts due to vibrational transitions, enough to be detected by a high-resolution spectrometer. In this way, it was possible to evaluate the chlorine isotopes as Al35Cl and Al37Cl with HR CS MAS.

Q: How is a typical day in your lab?

A: The first “experiment” of the day is coffee brewing. I usually organize everything that I need one day after, because we have two spectrometers for 10 people. When I use the instrument, I begin at 8 a.m. and there is no limit to end: sometimes at 5 p.m., sometimes at 10 p.m. I collect my data and process it the next day. We generally have lunch around 12 p.m. and use our free time to talk about everything, mostly nonsense subjects. Occasionally, I am responsible to do the maintenance of the spectrometers. Once in a month, we discuss our results with our supervisor.

Q: What common activities are organized in your research group?

A: We organize birthday parties in our laboratory, with junk food, soda, beer, and a cake. There are two barbecues each year: at the end of the year and at our supervisor birthday. We go out when someone publishes a paper, and the first author decide where the celebration is going to take place. In my case, always a bar.

Q: What app/programs do you typically use?

A: I usually write with Microsoft Word, although I also use LaTeX for some academic purposes. I like Microsoft Excel for data evaluation and/or processing, but Origin is my main choice for plotting graphs and spectra. Finally, but no less important, I use Microsoft PowerPoint for presentations.

Q: How do you search for scientific information? How do you manage your bibliography?

A: I search in Web of Science, Scopus, Science Direct, and Google Scholar. Sometimes I look directly in the journal sites, such as JAAS. I prefer to organize my bibliography in my computer folders, although I am beginning to use Mendeley to help me.

Q: What are your views on JAAS? Which type of articles do you prefer? Do you miss some content?

A: I have learned with Dr. da Veiga that JAAS is our first option for publication in atomic spectrometry. I always find interesting papers about this field, where my preferred ones are AAS and ICP techniques. I really like JAAS reviews, which are complete and straightforward to the subject.

Q: What do you like and dislike the most about your work?

A: I love working with analytical equipment and understanding their components. I want to know what they really can do and explore all the possibilities. It is funny because we usually do not have all the tools required; therefore, this topic is barely an option! I like my research group, in which I can talk about academic issues as well as tell jokes. I believe good relations are key to move the research forward. Finally, I enjoy when there are problems to be fixed, because I always learn something new while I try to fix them. However, I do not like them when they appear at 7 p.m. I feel disappointed when I work with people that does not want to learn.

Q: What do you expect to be doing in 5 years time?

A: That is a difficult question! I do not usually think too much in the future, because it is unpredictable. Generally, I prefer to stay focused on the present time and then I see which doors will be open. Although there are possibilities in large companies, I prefer academic research. Therefore, I would like to be a university researcher.

Q: What do you enjoy doing when you are not in the lab?

A: Everything related to beer, from brewing to drinking it. I have to learn much more about this beautiful and elegant beverage, therefore I am always trying to read about it or talk with people who knows this art. Origami (paper folding) has a special place in my hobbies, although I would like to practice it more than I usually do. I also like videogames and TV shows.

Surely, Breaking Bad. Thanks a lot, Flávio!

Have a look at Flávio recent articles in JAAS:

Chlorine isotope determination via the monitoring of the AlCl molecule by high-resolution continuum source graphite furnace molecular absorption spectrometry–a case study

FV Nakadi, M da Veiga, M Aramendía, E García-Ruiz, M Resano

Journal of Analytical Atomic Spectrometry, 2015, Advance article

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JAAS Emerging Investigator Lectureship winners announced

JAAS, 2014, Issue 1We are delighted to announce the winners of the inaugural JAAS Emerging Investigator Lectureship. Launched to coincide with the 30th anniversary of the journal, the lectureship will be awarded annually from 2015 to recognise and support an emerging scientist working in the area of atomic spectrometry in the early stages of their independent career.

With so many exceptional and highly deserving nominations, it was decided to award the JAAS Emerging Investigator Lectureship to two winners this year.

Congralutaions to Gerardo Gamez (Texas Tech University) and Lara Lobo Revilla (University of Oviedo)!

Lectureship award details

As a winner of the lectureship, both Gerardo and Lara will be able to present their research at a relevant high-profile international meeting and receive a contribution of up to £1000 each to cover associated travel and accommodation costs. They will be awarded a certificate and invited to contribute a paper to JAAS.

You can read more about eligibility and the selection process in the call for nominations post.

We will be posting more information about our winners soon!

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Join up with JAAS at the 6th Asia-Pacific Winter Conference in Xiamen, China

Will you be joining us in Xiamen later this month?

If so, on behalf of the organisers and JAAS Editorial Board, we would like to invite you to submit an article for a themed issue in JAAS, on your work presented at the conference.

The submission deadline for the issue will be 15th July 2015. Accepted papers will be published online as advanced articles as soon as they are ready. The issue will be published online and in print in early 2016. All authors will receive a PDF of their article and a print copy of this issue when it is published. There will be no upper limit on the number of papers published in the themed issue.

We welcome the submission of communications, full papers and technical notes for consideration in the issue, and all articles will be subject to the usual high standards of the journal through peer-review. If you are interested in writing a review article for the issue, then please do not hesitate to contact me by email. We will also have a JAAS 30th Anniversary Event on the Friday night, so please do come and speak to me!

Articles should be submitted through the JAAS website, and we kindly ask all authors to indicate in their covering letter that their article is for consideration in the APWC 2015 issue. Further details about what we have to look forward to can be found on the conference website.

2015 Asia-Pacific Winter Conference (2015 APWC), Xiamen, China
May 19-22, 2015

Take a look at some of the papers published in the themed issue from the 2012 Asia Pacific Winter Conference, held in Jeju Island, South Korea

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