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HOT Articles in Analytical Methods

Take a look at our new hot articles just published in Analytical Methods. These papers are all free to read until January 6th 2014. Enjoy the reading!

Multianalytical approach to explain the darkening process of hematite pigment in paintings from ancient Pompeii after accelerated weathering experiments
Maite Maguregui, Kepa Castro, Héctor Morillas, Josu Trebolazabala, Ulla Knuutinen, Rita Wiesinger, Manfred Schreiner and Juan Manuel Madariaga
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41741G, Paper

A new method to determine the thickness of platinum nanofilm simply by measuring its electrical resistance
Yujing Sun, Zhiwei Wen, Fugang Xu, Yue Zhang, Yan Shi, Haichao Dai and Zhuang Li
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41488D, Communication

A real-time cell-electronic sensing method for comparative analysis of toxicity of water contaminants
Haiying Du, Jinhua Li, Birget Moe, Claire F. McGuigan and Xing-Fang Li
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41686K, Paper

Magnetic imprinted surface enhanced Raman scattering (MI-SERS) based ultrasensitive detection of ciprofloxacin from a mixed sample
Zhinan Guo, Lei Chen, Haiming Lv, Zhi Yu and Bing Zhao
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY40866C, Paper

Synthesis, characterization and adsorption performance of molecularly imprinted nanoparticles for tripterine by precipitation polymerization
Yuan Liu, Guifeng Zhang, Lihong Deng, Jiandu Lei, Lianyan Wang and Jing He
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41772G, Paper

Selection, identification and application of a DNA aptamer against Staphylococcus aureus enterotoxin A
Yukun Huang, Xiujuan Chen, Yu Xia, Shijia Wu, Nuo Duan, Xiaoyuan Ma and Zhouping Wang
Anal. Methods, 2014, Advance Article
DOI: 10.1039/C3AY41576G, Paper

Multianalytical approach to explain the darkening process of hematite pigment in paintings from ancient Pompeii after accelerated weathering experiments

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Detecting iron the smart way

Spanish scientists have developed a way to quantitatively measure the amount of iron in a solution using a colour changing material and photos taken on a smartphone. Detecting iron the smart way

Iron is present in almost every aspect of our lives but an excess, known as iron overload, can cause significant long term effects ranging from liver damage to arthritis as a result of iron deposition in organs or joints. As such, the amount of iron in a variety of environments needs to be carefully monitored.

Unlike traditional quantitative techniques, which require removing samples to the lab for assessment by trained specialists, the new approach devised by José Miguel García and colleagues at the University of Burgos can return a result within 15 minutes. Central to the technique is 8-hydroxyquinoline, a particularly stable iron chelator, which is immobilised on a polymer disk and will change colour depending on the amount of iron chelated to it.

To read the full article, please visit Chemistry World.

Solid sensory polymer substrates for the quantification of iron in blood, wine and water by a scalable RGB technique
Saúl Vallejos, Asunción Muñoz, Saturnino Ibeas, Felipe Serna, Félix Clemente García and José Miguel García
J. Mater. Chem. A, 2013, Advance Article
DOI: 10.1039/C3TA12703F

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Eye spy cyanide

The colour of cyanide poisoning is purple, according to researchers in Switzerland who have developed a method that enables them to quickly detect blood cyanide levels through a simple colour change.

The two-step method to detect cyanide. (A) Adding a chemosensor to a blood sample, followed by extracting the purple chemosensor–cyano complex from the sample. (B) Washing the column with water

The two-step method to detect cyanide. (A) Adding a chemosensor to a blood sample, followed by extracting the purple chemosensor–cyano complex from the sample. (B) Washing the column with water

Cyanide poisoning as a result of smoke inhalation can have serious or fatal consequences unless an antidote is rapidly administered. Current methods for determining cyanide poisoning, including microdiffusion, microdistillation and liquid chromatography-mass spectrometry detection, can take up to an hour to give results and are not suitable for point-of-care settings.

Read the full article in Chemistry World online.

Rapid visual detection of blood cyanide
Christine Männel-Croisé and Felix Zelder
Anal. Methods, 2012, Advance Article
DOI: 10.1039/C2AY25595B

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Anion detection method to help police fight crime

 

Molotov cocktail

Chemical ignition Molotov cocktails consist of a flammable liquid and sulfuric acid and potassium chlorate in a glass bottle. The mixture is set alight by the reactants’ reaction on smashing the bottle

Researchers in Spain have developed a fast, non-hazardous method of identifying the anions present in improvised incendiary devices (a type of petrol bomb). This information will be important to police officers, as knowing the components of the original device could potentially help lead to the suspects involved.

Carmen García-Ruiz of the University of Alcalá, Madrid, and her co-workers studied a particular type of device – so-called chemical ignition Molotov cocktails (CIMCs), which consist of a flammable liquid (typically petrol) along with sulfuric acid and potassium chlorate in a glass bottle. Rather than needing to be lit by the thrower, the exothermic reaction of these ingredients on contact sets the mixture alight.

Read the full article in Chemistry World.

Qualitative Determination of inorganic anions in incendiary device residues by capillary electrophoresis
Carlos Martín-Alberca, Jorge Sáiz, José Luis Ferrando and Carmen Garcia Ruiz
Anal. Methods, 2012, Accepted Manuscript

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