Issue 3 online

JAAS, 2011, 26(3):465-636

Issue 3 has just been published online, so head over to the JAAS homepage to take a look.  On this month’s cover, work by Thomas Pettke et al. to determine lead isotope ratios is highlighted.

They present an analytical protocol for measuring isotope ratios on minute analyte quantities by multiple-collector ICP-MS in fast transient signal mode.  They say that this has great potential for applications to geochemical, archaeological, environmental and possibly biochemical problems.

Quantification of transient signals in multiple collector inductively coupled plasma mass spectrometry: accurate lead isotope ratio determination by laser ablation of individual fluid inclusions
Thomas Pettke, Felix Oberli, Andreas Audétat, Uwe Wiechert, Caroline R. Harris and Christoph A. Heinrich
J. Anal. At. Spectrom., 2011, 26, 475-492
DOI: 10.1039/C0JA00140F

Read the article for free for the next 6 weeks.

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Metallomics 2011 Reminder: February 28 Deadline

(Carsten Engelhard) The deadline for abstract submissions to the Third International Symposium on Metallomics  is February 28.

Metallomics 2011

The conference will be held from June 15 – 18, 2011 in Muenster, Germany.  After two successful conferences in Japan and the USA,  it is the first time that the conference will be held in Europe. Chairman Uwe Karst (University of Muenster, Germany) and co-chair Michael Sperling (EVISA) are assembling a program that will highlight the interdisciplinary character of the science involved in answering questions about the abundance of metal and metalloid species in biological systems. A number of distinguished experts will present the state-of-the-art in metallomics research.

Submissions can be made online by February 28, 2011 at the conference website: http://www.metallomics2011.org. The submission deadline for late poster contributions is March 31, 2011.

Muenster is a wonderful place to visit and was awarded the 2004 International Award for Liveable Communities. Historic buildings from nine centuries, a lot of opportunities for shopping/dining, and approx. 250 km of bicycle tracks make the city a truly unique experience.

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HOT Article: Insights into the corrosion resistance of ancient phosphorus-containing iron

X-ray absorption spectroscopy study of the various forms of phosphorus in ancient iron samples Ancient phosphorus-containing iron-based alloys are often reported to be strongly resistant toward corrosion, but the mechanisms of this protection have not yet been explained. In order to better understand the role of this element, in the conditions of atmospheric corrosion, Judith Monnier and co-workers in France used micro-XANES spectra to highlight phosphorus distribution and speciation in two ancient iron-based samples.

Interested in knowing more? Read the full article here; free until March 18th!

X-ray absorption spectroscopy study of the various forms of phosphorus in ancient iron samples
Judith Monnier, Delphine Vantelon, Solenn Reguer and Philippe Dillmann
J. Anal. At. Spectrom., 2011, Advance Article
DOI: 10.1039/C0JA00247J

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European Winter Conference 2013

To be held in the historic city of Krakow

The next European Winter Conference on Plasma Spectrochemistry will be held 10-15 February 2013 in Krakow, Poland.

Chair of the meeting will be JAAS Editorial Board member Joanna Szpunar from the Laboratory of Bio-Inorganic and Environmental Analytical Chemistry at CNRS, Pau, France.  She will be supported by Co-Chair Paweł Kościelniak from the Faculty of Chemistry at the Jagiellonian University, Krakow.

Krakow is known as one of the oldest and most beautiful cities in Central Europe, and is listed as a UNESCO World Heritage Site.  The EWCPS is being organised with the support of the Polish Academy of Sciences, the Polish Society of Chemistry, the President of the City of Krakow and the Rector of the Jagiellonian University.

To find out more, visit www.chemia.uj.edu.pl/ewcps and keep an eye on JAAS News – we’ll give you more updates as we have them.

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The Future of Plasma-Based Analytical Instrumentation

European Winter Conference 2011

EWC 2011

(Carsten Engelhard) At the European Winter Conference Ryszard Lobinski (Laboratory of Analytical Bioinorganic and Environmental Chemistry, University of Pau, France) hosted a round table discussion on the current status and future of plasma-based analytical instrumentation.  Participants from instrument manufactures included Dirk Ardelt (Spectro Analytical Instruments), Kaveh Kahen (Perkin Elmer), Paul Neal (Thermo Fisher Scientific), Andrew Ryan (Bruker), and Steven Wilbur (Agilent Technologies).

Four major topics were covered: a) current challenges in plasma source instrumentation, b) how to choose a plasma source spectrometer, c) plasma source spectrometry and society: new markets and applications, and last but not least, d) teaching and training in ICP spectroscopy.

During an enjoyable one-hour discussion, it was stated that plasma-based analytical instrumentation has come a long way since its first introduction, but that there is still a lot of room for improvement.  In the future, it will presumably become more important to improve the absolute sensitivity, to reduce the required sample size, and to detect major constituents next to ultra trace elements with high precision.  Moreover, environmental considerations and consumer needs might require the reduction of carbon footprint, and the use of low gas flow or miniaturized plasma-based analytical instrumentation.

It is clear that an interesting future lies ahead of plasma-based analytical instrumentation.  The ideal analytical instrument that provides us with both atomic and molecular information with high precision and high sensitivity is still a vision. However, instrument manufactures as well as university researches are continuously working on the improvement of existing and the development of new instrumentation. There is still a lot to be done. Lets get started!

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HOT Article: Novel method of X-ray fluorescence microanalysis of metallic objects

Reduction of surface effects and relief reconstruction in X-ray fluorescence microanalysis of metallic objects This HOT article by T. Trojek from the Czech Technical University in Prague reports on relief imaging and an improved method of quantitative evaluation in microscopic X-ray fluorescence analysis of metallic objects.  This paper introduces a simple but brilliant idea on how to extract quantitative data from rather not so easily quantifiable measurements and has far reaching applications.

Interested in knowing more?  Read this HOT Article for free until March 11th.

Reduction of surface effects and relief reconstruction in X-ray fluorescence microanalysis of metallic objects
T. Trojek
J. Anal. At. Spectrom., 2011, Advance Article
DOI: 10.1039/C0JA00187B

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CSI XXXVII Conference Call For Papers: April 30 Deadline

CSI

The Colloquium Spectroscopicum Internationale XXXVII will be held August 28-September 2, 2011 in Buzios, Brazil.  This is quite an auspicious occasion, since it will be the first time the CSI conference will be held in a Latin American country.  Chairman Reinaldo C. Campos (Department of Chemistry, PUC-Rio, Brazil) and his co-organizers are assembling what is sure to be a great conference – and they have issued the first call for papers.

Submissions can be made online by April 30, 2011 at the conference website: http://www.csixxxvii.org/index.php.  Buzios is a wonderful locale, with great beaches, nightlife, and food—and there is sure to be alot of great science to boot!

The Beaches of Buzios

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Rebeca Valledor wins Payling Award for best work in Glow Discharge

Award winner Rebeca Valledor with Prof. Nerea Bordel

The European Winter Conference is the traditional home of the Richard Payling Prize, which given to the best contribution on the topic of glow discharge spectrochemistry presented at that conference.  The 2011 award winner is Rebeca Valledor from the University of Oviedo, Spain.

Rebeca presented a poster entitled “Spatially and Temporally Resolved Studies of the Optical Emission in a Pulsed Radiofrequency Glow Discharge” (PC-052) in which she and her coworkers studied the temporal evolution of a pulsed RF glow discharge through spatially resolved spectroscopy, permitting them to deduce ionization and excitation mechanisms that are of critical importance in the design of a glow discharge source for mass spectrometry.

An advanced article just published online in JAAS (Valledor, R., Pisonero, J., Niels, T., and Bordel, N., Spatial characterization of pressure-based plasma regimes in a radio frequency glow discharge by using optical emission spectroscopy, Advance Article) provides a good preview of the work.

The award was sponsored by Horiba Jobin-Yvon, Spectruma Analytik GMbH, Tofwerk AG, Leco Inc., ThermoFischer, and nu Instruments.  Well done Rebeca!

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2011 Hot Plasma Party achieves EPIC proportions

In addition to a great scientific program, the European Winter Conference is known for its social aspects–and perhaps most prominent in this program is the ‘Hot Plasma Party‘ traditionally held on the eve of the first full day of the conference.  This year, the organizing committee took the conferees to the San Valero Winery outside of Zaragoza for dinner and dancing,  with the stipulation that the dress code include some red and black.  After a wonderful dinner, the organizing committee had a surprise planned: None other than Mr. Tom Jones!

Mr Sal Starr and Company entertain the conferees

Actually, this was Salvatore Starr–an ardent follower of Mr. Jones who sounds and looks a lot like Tom–and Salvatore puts on a show with just as much energy as Tom ever did.  You can tell from the pictures that a great deal of fun resulted.  I will not post any pictures that might embarrass anyone besides myself (and my good friend Jorge Pisonero).  Two things occur to me: First, somebody should setup a flickr account to share these photos- they are great; and second- somebody should organize something similar for the US and Asia-Pacific conferences.  These are too much fun!

Mr Jones?

Sal, Steve, and Jorge

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Alfredo Sanz-Medel and Frank Vanhaecke share the 2011 European Plasma Award

The 2011 European Plasma Award was presented to both Professor Alfredo Sanz-Medel (Univeristy of Oviedo, Spain) and Prof. Frank Vanhaecke (Ghent University, Belgium) for their significant contributions to plasma spectrochemistry. The European Plasma Award is sponsored by Agilent Technologies.

Prof. Alfredo Sanz-Medel

Prof. Sanz Medel presented an award lecture entitled ” Mass Spectrometry for isotopes, elements, molecules, and nanoparticles“,  Prof. Vanhaecke then followed with a lecture entitled “Having fun at the scientific playground: Isotope ratio applications using (multi-collector) ICP-mass spectrometry“.

Prof. Frank Vanhaecke

It goes without saying that both lecturers were excellent and well received, but perhaps the most interesting aspect of the award ceremony was the evident esteem in which the award winners held one another and the philosophy of research that each touched upon (and that is largely held in common between them).  These are certainly two excellent teachers, researchers, and colleagues–and the award is richly deserved in each case!

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