Top ten most accessed articles in February

This month sees the following articles in JAAS that are in the top ten most accessed:-

Atomic spectrometry update. Environmental analysis 
Owen T. Butler, Warren R. L. Cairns, Jennifer M. Cook and Christine M. Davidson 
J. Anal. At. Spectrom., 2013,28, 177-216 
DOI: 10.1039/C2JA90077G  

Atomic spectrometry update—X-ray fluorescence spectrometry 
Margaret West, Andrew T. Ellis, Philip J. Potts, Christina Streli, Christine Vanhoof, Dariusz Wegrzynekf and Peter Wobrauschek 
J. Anal. At. Spectrom., 2012,27, 1603-1644 
DOI: 10.1039/C2JA90045A  

Silver nanoparticle characterization using single particle ICP-MS (SP-ICP-MS) and asymmetrical flow field flow fractionation ICP-MS (AF4-ICP-MS) 
Denise M. Mitrano, Angela Barber, Anthony Bednar, Paul Westerhoff, Christopher P. Higgins and James F. Ranville 
J. Anal. At. Spectrom., 2012,27, 1131-1142 
DOI: 10.1039/C2JA30021D  

Limitations of the exponential model for the correction for mass discrimination effects during isotope ratio measurements by MC-ICPMS. Demonstration with Sr at 5–15 µL min-1 continuous liquid flow rates 
E. Paredes, J. L. Todolib and C. R. Quétel 
J. Anal. At. Spectrom., 2013,28, 327-333 
DOI: 10.1039/C3JA30210E  

Reproducibility of CIGS thin film analysis by laser-induced breakdown spectroscopy 
Jung-Hwan In, Chan-Kyu Kim, Seok-Hee Leea and Sungho Jeong 
J. Anal. At. Spectrom., 2013,28, 473-481 
DOI: 10.1039/C3JA30298A  

Atomic spectrometry update. Industrial analysis: metals, chemicals and advanced materials 
Simon Carter, Andy S. Fisher, Michael W. Hinds and Steve Lancaster 
J. Anal. At. Spectrom., 2012,27, 2003-2053 
DOI: 10.1039/C2JA90058K  

Determination of prostate-specific antigen (PSA) tagged with TiO2 nanoparticles using ICP-MS 
H. K. Choa and H. B. Lim 
J. Anal. At. Spectrom., 2013,28, 468-472 
DOI: 10.1039/C3JA30299G  

Speciation of selenium in cells by HPLC-ICP-MS after (on-chip) magnetic solid phase extraction 
Beibei Chen, Bin Hu, Man He, Qian Huang, Yuan Zhanga and Xing Zhang 
J. Anal. At. Spectrom., 2013,28, 334-343 
DOI: 10.1039/C2JA30280B  

Isotope ratio measurements by MC-ICPMS below 10 µL min-1 under continuous sample flow conditions. Exploring the limits with strontium 
E. Paredes, D. Goitom Asfahaa and C. R. Quétel 
J. Anal. At. Spectrom., 2013,28, 320-326 
DOI: 10.1039/C2JA30209H  

Accurate determination of S in organic matrices using isotope dilution ICP-MS/MS 
Lieve Balcaen, Glenn Woods, Martín Resanoc and  Frank Vanhaecke 
J. Anal. At. Spectrom., 2013,28, 33-39 
DOI: 10.1039/C2JA30265A  

Why not take a look at the articles today and blog your thoughts and comments below.

Fancy submitting an article to JAAS? Then why not submit to us today or alternatively email us your suggestions.

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Allan Ure Bursary – Call for Applications

Allan Ure Bursary – Call for Applications
DEADLINE: 31st May 2013

The Allan Ure Bursary is awarded on an annual basis, alternately by the Atomic Spectroscopy Group of the Analytical Division of the Royal Society of Chemistry (ASG, AD, RSC) and the Atomic Spectrometry Updates (ASU) Editorial Board.

The award is presented to a scientist, at the start of their career, who the adjudicators believe has made a significant contribution to knowledge in the area of the application of atomic spectrometry to environmental science. The successful applicant will receive £500 to help with any expenses that may be of benefit to their career.

Who can apply?
Applicants need not be specialised analytical chemists and may come from fields as diverse as geology, biology, oceanography, geography and environmental science. They will, however, have to demonstrate that they use atomic spectrometry on a regular basis for their work. The scope of the Atomic Spectrometry Update – Environmental Analysis, published each year in the February issue of the Journal of Analytical Atomic Spectrometry may be taken as guidance.

Applications
Applications should be made electronically and consist of the applicant’s Curriculum Vitae plus a covering letter which clearly states how the bursary will be used and how the applicant believes this will benefit their career. The name of one referee (normally the applicant’s line manager) who is familiar with the applicant’s recent work should also be provided.

Applications may be submitted to ASG electronically to Dr A Fisher, afisher@plymouth.ac.uk

Further Information
Details of past winners and further information can be found on the ASG Website.

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Mars: Where the Sky is Orange

Sirven et al. featured on the front cover of JAAS, 2007, Issue 12

Yesterday the Royal Society of Chemistry had the pleasure to meet the driver of the Mars Curiosity rover Paolo Bellutta who revealed the secrets of Mars one year after the first ‘landing’ in 2012.

You might remember the paper published in 2007 in JAAS about ChemCam, the powerful instrument now functional part of the Mars Science Laboratory Curiosity rover used to study the red planet.

ChemCam uses laser induced breakdown spectroscopy (LIBS) to remotely analyse the surface of Mars looking into the chemistry of its rocks.

Jean-Baptiste Servien and colleagues at CEA Saclay, France, introduced the three chemometric approaches used by ChemCam to study the rocks on the surface of Mars in the paper entitled Feasibility study of rock identification at the surface of Marsby remote laser-induced breakdown spectroscopy and three chemometric methods.

Mars Curiosity rover on the red planet

Last August, Curiosity successfully landed at Gale Crater on the planet Mars. Paolo Bellutta, Rover’s driver from NASA’s Jet Propulsion Laboratory, explained what is behind a one-ton vehicle that is able to land in such a hostile place where the wind runs at 400Km/h, the temperature reaches -90°C and the sky turns orange.

How do we drive on Mars? And what are we doing on Mars ? To know everything about the Mars Mission watch the video soon available on The Reaction website.

Free for you until May 13th: Feasibility study of rock identification at the surface of Mars by remote laser-induced breakdown spectroscopy and three chemometric methods
Jean-Baptiste Sirven, Béatrice Sallé, Patrick Mauchien, Jean-Luc Lacour, Sylvestre Maurice and Gérard Manhès
J. Anal. At. Spectrom., 2007, 22, 1471-1480
DOI: 10.1039/B704868H

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Reconstructing how the Romans made glass

Man has been making glass since the third millennium BC and during the manufacture of ancient glass, antimony, in a metal or mineral form, was added to make it colourless or opaque.

Different antimony ores have slightly different antimony isotope ratios and researchers in Belgium and the UK have developed an inductively-coupled plasma mass spectrometry (ICP-MS) method to detect and quantify these tiny differences. By analysing samples of Roman glass, the team hope to uncover clues about how the glass was made and the geographical provenance of the raw materials.

 

To read the full article please visit Chemistry World.

Isotopic analysis of antimony using multi-collector ICP-mass spectrometry for provenance determination of Roman glass
Lara Lobo,Patrick Degryse,Andrew Shortland and Frank Vanhaecke
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA50018G

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JAAS Issue 5 now online!

The latest issue of JAAS  is now online! Take a look at our great covers and read all about the new research behind them. We also have some HOT papers free for you to enjoy.

The outside front cover shows the work of JAAS Editorial Board Member Martín Resano and colleagues at the University of Zaragoza, Spain. In their paper, the researchers propose a direct analysis of carbon nanotubes using solid sampling high-resolution continuum source graphite furnace atomic absorption spectrometry.

Simultaneous determination of Co, Fe, Ni and Pb in carbon nanotubes by means of solid sampling high-resolution continuum source graphite furnace atomic absorption spectrometry
Martín Resano ,  Eduardo Bolea-Fernández ,  Engracia Mozas ,  María R. Flórez ,  Patricia Grinberg and Ralph E. Sturgeon
J. Anal. At. Spectrom., 2013,28, 657-665
DOI: 10.1039/C3JA30377B

Our inside front cover showcases work previously featured in our recent JAAS Web Collection on Atomic Spectrometry in Biomedical Science.

Kaori Shigeta at the Tokyo Institute of Technology and colleagues at BAM federal Institute for Materials Research and Testing, Germany, report the sample introduction of single selenized yeast cells by microdroplet generation into a ICP-sector field mass spectrometer for label free detection of trace elements.

Sample introduction of single selenized yeast cells (Saccharomyces cerevisiae) by micro droplet generation into an ICP-sector field mass spectrometer for label-free detection of trace elements
Kaori Shigeta ,  Gunda Koellensperger ,  Evelyn Rampler ,  Heike Traub ,  Lothar Rottmann ,  Ulrich Panne ,  Akitoshi Okino and Norbert Jakubowski
J. Anal. At. Spectrom., 2013,28, 637-645
DOI: 10.1039/C3JA30370E

Along with our new covers, here are the HOT papers featured in this issues. These articles will be free to read until May 13th. Have a read now!

Application of a micro-droplet generator for an ICP-sector field mass spectrometer – optimization and analytical characterization
Kaori Shigeta ,  Heike Traub ,  Ulrich Panne ,  Akitoshi Okino ,  Lothar Rottmann and Norbert Jakubowski
J. Anal. At. Spectrom., 2013, 28, 646-656
DOI: 10.1039/C2JA30207A

235 U–231Pa age dating of uranium materials for nuclear forensic investigations
Gary R. Eppich ,  Ross W. Williams ,  Amy M. Gaffney and Kerri C. Schorzman
J. Anal. At. Spectrom., 2013, 28, 666-674
DOI: 10.1039/C3JA50041A

Isotopic analysis of Cu in serum samples for diagnosis of Wilson’s disease: a pilot study
Maite Aramendía ,  Luis Rello ,  Martín Resano and Frank Vanhaecke
J. Anal. At. Spectrom., 2013, 28, 675-681
DOI: 10.1039/C3JA30349G

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Broad bobbin collar too fashionable?

While X-ray fluorescence (XRF) spectroscopy is a well-established technique for the investigation of paintings, the apparatus used are usually custom built and not widely available. Now, Matthias Alfeld and colleagues have developed a portable macro XRF spectrometer to look at paintings in situ.

The team used the device to look at a portrait by Govert Flinck, a Dutch painter who was a protégé of the great Rembrandt. Interestingly, they found that originally the subject was painted wearing a broad bobbin lace collar and long lace cuffs but this was toned down for the final version, possibly because it was too trendy.

Govert Flinck, Portrait of Dirck Jacobsz. Leeuw and elemental distribution images of the painting.

 To read the full article please visit Chemistry World.

A mobile instrument for in situ scanning macro-XRF investigation of historical paintings
Matthias Alfeld ,  Joana Vaz Pedroso, Margriet van Eikema Hommes, Geert Van der Snickt, Gwen Tauber, Jorik Blaas, Michael Haschke, Klaus Erler, Joris Dik and Koen Janssens
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA30341A

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2015 European Winter Conference on Plasma Spectrochemistry

Those of you who attended the Closing Ceremony of the recent 2013 Winter Conference on Plasma Spectrochemistry in Krakow, will have heard that the RSC was planning to host the 2015 European Winter Conference in Glasgow, with Professor Joerg Feldmann from University of Aberdeen as Chair.

You may also have seen that nominations to host the conference in 2015 are now open again, and you could be wondering why this is.

We are sad to say that our submitted bid was not felt to be suitable by the Continuation Committee, and so we have respectfully acknowledged their decision. However we would like to take this opportunity to assure you that we did not withdraw our support, and that it has always been our intention to act in support of the community and in accordance with your wishes.

We became involved in the bidding process because after the Zaragoza conference, we were approached by members of the community who asked if the RSC would be willing to consider supporting a bid to bring the conference back to the UK after 20 years. Following careful consideration of the Conference Constitution, we consulted with the Chair of the Krakow conference to ask whether our involvement as a society would be possible. No concerns were raised with us that were not addressed in our bid and in discussions with the Committee, prior to the awarding of the bid to Glasgow.

After this initial agreement made in Krakow, the Committee still had serious concerns regarding aspects of the bid, including the level of the involvement of the RSC, such that they do not believe it to be in the best interest of the community for us bring the Winter Conference back to the UK in 2015.

The RSC has a long history of involvement with the atomic spectrometry community and the Winter Conferences.  Our intention with the Glasgow bid was and will continue to be, to support the community in whatever way we can. It goes without saying that we look forward to working with and supporting you in the future.

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Hot Articles in JAAS!

New synthesis of silica nanoparticles

New synthesis of silica nanoparticles

Silica nanoparticles can now be easily developed and efficiently used in bioassays. This study just published in JAAS by Jung Aa Ko and H. B. Lim shows the design and optimisation of a new method for synthesis of core-shell nanoparticles doped with metal ions and dye together for particle tagging and monitoring.

Metal/dye-doped core-shell silica nanoparticles for potential use in bioassay
Jung Aa Ko and H. B. Lim
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA30373J

Precise measurements of platinum stable isotopes

Measuring platinum stable isotopes

Researchers at the Victoria University of Wellington, New Zealand, present the precise measurement of platinum (Pt) stable isotopes by multiple collector inductively coupled plasma mass spectrometry (MC-ICPMS) using two diffrerent double spikes. The authors explain that the 196Pt-198Pt spike is preferable for application to both natural terrestrial and extraterrestrial samples.

Platinum stable isotope ratio measurements by double-spike multiple collector ICPMS
John Creech ,  Joel Baker ,  Monica Handler ,  Martin Schiller and Martin Bizzarro
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA50022E

Both papers will be free to read until April 25th. Have a read now!

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Spectral interferences using Inorganic Mass Spectrometry

Analysis of Human urine after administration of Gd-based MRI contrast agents

Administration of Gd-based MRI contrast agents causes major spectral interferences during analysis of selenium (Se) and platinum (Pt) in urine.

The finding was reported in a new study led by Amy Steuerwald who carried out an epidemiological study on 619 urine specimens to determine Se and Pt using quadruple-based inductively coupled plasma mass spectrometry (Q-ICP-MS). Both Se and Pt were several orders of magnitude greater than the upper limit of the population reference ranges.

To read the full article, please access the link below. This paper will be free to read until April 12th.

Trace element analysis of human urine collected after administration of Gd-based MRI contrast agents: characterizing spectral interferences using inorganic mass spectrometry
Amy J. Steuerwald ,  Patrick J. Parsons ,  John G. Arnason ,  Zhen Chen ,  C. Matthew Peterson and Germaine M. Buck Louis
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA30331D

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Web Collection: Analytical Atomic Spectrometry in Biomedical Science

Check out the new JAAS web collection on Analytical Atomic Spectrometry in Biomedical Sciences!

All the JAAS papers included in this collection highlight the latest achievements in analytical atomic spectrometry and the applications of spectroscopy-based bioanalytical technology in clinics and biology.

To view the full list of articles, take a look at our Web Collection now!

Here are some interesting selected papers free for you to enjoy for the next four weeks. To read the full articles, please click on the links below:

Isotopic analysis of Cu for diagnosis of Wilson's disease

Isotopic analysis of Cu in serum samples for diagnosis of Wilson’s disease: a pilot study
Maite Aramendía ,  Luis Rello ,  Martín Resano and Frank Vanhaecke
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA30349G

Comparison of different chelates for lanthanide labeling of antibodies and application in a Western blot immunoassay combined with detection by laser ablation (LA-)ICP-MS
Larissa Waentig ,  Norbert Jakubowski ,  Simone Hardt ,  Christian Scheler ,  Peter H. Roos and Michael W. Linscheid
J. Anal. At. Spectrom., 2012,27, 1311-1320
DOI: 10.1039/C2JA30068K

A pilot study on the use of laser ablation-ICP-mass spectrometry for assessing/mapping the distribution of a drug and its metabolites across the body compartments of rats
Andrei Izmer ,  Deepti Gholap ,  Kathleen De Houwer ,  Filip Cuyckens and Frank Vanhaecke
J. Anal. At. Spectrom., 2012,27, 413-418
DOI: 10.1039/C2JA10343E

GFAAS for direct determination of gold in mice exposed to gold nanoparticles

Solid sampling high-resolution continuum source graphite furnace atomic absorption spectrometry to monitor the biodistribution of gold nanoparticles in mice tissue after intravenous administration
M. Resano ,  E. Mozas ,  C. Crespo ,  J. Briceño ,  J. del Campo Menoyo and M. A. Belarra
J. Anal. At. Spectrom., 2010,25, 1864-1873
DOI: 10.1039/C0JA00086H

Quantitative imaging of element spatial distribution in the brain section of a mouse model of Alzheimer’s disease using synchrotron radiation X-ray fluorescence analysis
Hua-Jian Wang ,  Meng Wang ,  Bing Wang ,  Xiang-Yu Meng ,  Yun Wang ,  Ming Li ,  Wei-Yue Feng ,  Yu-Liang Zhao and Zhi-Fang Chai
J. Anal. At. Spectrom., 2010,25, 328-333
DOI: 10.1039/B921201A

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