Archive for the ‘News’ Category

The Next Generation-Inteview with Morgana B. Dessuy

We continue this section by interviewing Morgana B. Dessuy, a very young, just appointed Professor at Universidade Federal do Rio Grande do Sul (UFRGS), Porto Alegre, BrazilMorgana works at the Laboratory of Trace Analysis, coordinated by Prof. Dr. María G.R. Vale.

Morgana Dessuy in her lab in Porto Alegre

Who or what inspired you to become a scientist?

At school I was always interested in Sciences. During high school, I decided to study Chemistry, after having read some articles about the role of a chemist in society.

Why did you choose your research group/University and what factors influenced your choice?

During my graduation, at Universidade Federal de Santa Maria, I was given the chance to work with different analytical techniques. At the end of my degree I decided to work with Atomic Absorption Spectrometry (AAS), which led me to do my TCC, which is a first supervised research work to conclude the graduation course, at the Laboratory of Trace Analysis at Universidade Federal do Rio Grande do Sul (UFRGS), coordinated by Prof. Maria Goreti R. Vale. This TCC work increased my interest in this technique even more; consequently I decided to take my Master and Doctorate in this area. Considering the fact that the Laboratory of Trace Analysis offers an adequate infrastructure for the development of my research, and that UFRGS is one of the best universities of Brazil, I chose to follow my studies there under the supervision and orientation Prof. Maria Goreti. During my PhD work I also had the opportunity to spend one year at the Institute of Analytical Chemistry of the Academy of Science of the Czech Republic in Prague under the supervision of Dr. Jiři Dědina in the frame of a sandwich program. This gave me the opportunity to work with other techniques, to know new people and a different culture, which contributed very much to increase my horizon, scientifically and personally.

Can you explain a bit the purpose of your current research activities?

My current research is based on the application of the AAS technique for the development of analytical methods. I am currently working on the development of analytical methods for the quantification of non-metals using High-resolution Continuum Source Graphite Furnace Molecular Absorption Spectrometry (HR-CS GF MAS). Besides this project, I have been developing another study related to the leaching of metals and metalloids from different food containers, particularly from pewter cups produced in Brazil.

How is a typical day in your lab?

I am not able to stay for a long time in the laboratory to make measurements, due to my recent activities as a Professor. Having to divide my time among giving classes, research and doing the paperwork, what I usually do is to plan the experiments and discuss the results with the students in the lab early in the morning and at the end of the afternoon when I finish my classes.

What common activities are organized in your research group?

Eventually we gather to make a barbecue or a happy hour to celebrate birthdays, presentation of final papers or the approval of a scientific project.

How do you search for scientific information? How do you manage your bibliography?

To make the bibliographic review I make use of the Web of Science. In addition, I usually access the websites of the main Journals in the field, to follow what is being published, and I save in folders, ordered by subject, those articles that I find relevant.

What are your views on JAAS? Which type of articles do you prefer? Do you miss some content?

JAAS is one of the most important Journals in the field of Atomic Spectrometry, being a reference for me since the beginning of my graduation. Nowadays, I wish there were more articles about sample preparation, as well as method development and applications involving AAS techniques, mainly using high-resolution continuum source AAS and high resolution continuum source molecular absorption spectrometry.

What do you like and dislike the most about your work?

I really like my work and I feel honored for being able to provide classes and carry out research activities simultaneously. I am happy with what I do. I do not really like the administrative paperwork, which is automatically inserted in my duties. Having to administrate money for my research and face bureaucracy and delay for the purchase of material/reagents is really annoying.

What do you expect to be doing in 5 years time?

I have recently reached a position, which I have aimed for a long time: the one of being a Professor at UFRGS. In five years time I hope to have acquired the potential to widen the structure of the Laboratory of Trace Analysis and to be satisfied with the research developed during this time. Besides that, I hope to contribute to the formation of graduate and post-graduate students.

What do you enjoy doing when you are not in the lab?

I really like going out with my friends or going to a park on the weekends. I also like reading a lot of books of general literature.

Thanks for sharing your views with us, Morgana, and congratulations on your recent position!

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Gordon F. Kirkbright Bursary Award, 2014

The Gordon F. Kirkbright bursary award is a prestigious annual award that enables a promising student/non-tenured young scientist of any nation to attend a recognised scientific meeting or visit a place of learning.
The fund for this bursary was established in 1985 as a memorial to Professor Gordon Kirkbright in recognition of his contributions to analytical spectroscopy and to science in general. Although the fund is administered by the Association of British Spectroscopists (ABS) Trust, the award is not restricted to spectroscopists.

Applications are invited for the 2014 Gordon Kirkbright Bursary.

For further information contact John Chalmers at, email: vibspecconsult@aol.com

The closing date for entries is 31 December 2013.

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The Next Generation-Interview with Luca Flamigni

We are starting a new section in JAAS News in which we will try to find out the views of the younger generation of atomic spectroscopists. Today, we are publishing an interview with Luca Flamigni, who is currently a PhD student in Detlef Gunther’s group at ETH Zürich (Switzerland).

Luca Flamigni in his lab at ETH Zürich

Who or what inspired you to become a scientist?

I have always been interested in technical and scientific aspects of life and nature. I think I inherited this curiosity from my father, who is a biologist and teaches science and mathematics in a secondary school.

Why did you choose your research group/University and what factors influenced your choice?

After my MSc in chemistry at ETH, I decided to pursue a PhD in analytical chemistry. At that point, I had done three projects in analytical chemistry at ETH and I was convinced that mass spectrometry was appealing the most to me. After being accepted as a student by Prof. Günther, I had no more doubts that analytical chemistry was my field of interest and joined his group for micro and trace analysis. ETH has a great infrastructure, is a world-class university, and is not too far from my home town.

Can you explain a bit the purpose of your current research activities?

My work is dedicated to a better understanding of the processes occurring inside the inductively coupled plasma (ICP) for mass spectrometric analysis of laser-produced aerosols. The theoretical considerations and experimental results obtained during my thesis will lead to new quantification strategies and instrumental developments on the ICP side.

How is a typical day in your lab?

I have two different typical days, depending on whether I am doing measurements or working at the computer. When I work in the lab, I usually try to get everything up and running until lunch, which is very early – at around eleven – in our group. Then, in the afternoon, I first run the most important experiments, which are on my schedule. If there is time left, I continue with what I thought of during the first experiments. If I am working in the office, I usually do repetitive, bureaucratic and easier tasks in the morning, when I tend to be less creative, then I do all the programming and interpretation in the afternoon.

What common activities are organized in your research group?

Our group is known for its good social life. For every accepted manuscript, the first author invites all group members for a drink after work. A few times every semester we meet for a barbecue or a drink for special occasions and when we have visitors. Other than that, every two years there is a group retreat, where we gather somewhere for two or three days. Last time we went to a castle close to the Lake Constance in the North-East of Switzerland. It was really a picturesque place to visit.

What app/programs do you typically use?

Everybody here in the lab knows me as an ImageJ enthusiast. ImageJ is a free piece of software used for image processing and microscopy. I do most of my work with it and have a folder full of useful macros to perform many tasks, such as size determination of micro-droplets, evaluation of SEM pictures, particle tracking etc. Beside the typical programs (Microsoft Office, Origin, SigmaPlot, LabVIEW, Adobe Photoshop), I am sometimes programming in Java using the NetBeans IDE and I recently started to experiment with Comsol for the simulation of flow systems.

How do you search for scientific information? How do you manage your bibliography?

I read at least twice a week the “recent articles” pages of JAAS and of the other analytical chemistry journals. When I find something interesting, I add the bibliographic information to Zotero, which is a browser plugin. When I do bibliographic research for a paper, I use SciFinder, which is a very powerful tool provided by the ETH library. I also use Google Scholar, which is helpful to retrieve information from outside the field of analytical chemistry. When I write a paper, I import the bibliography I have in Zotero into EndNote, which integrates well with Microsoft Word.

Which type of articles do you prefer?

We are forced to read broader, but clearly I like the articles on ICP-MS. Many of them are dealing with laser ablation and I find them always very interesting. Recently, I started to pay more attention also to the LIBS articles. LIBS is having a sort of revival, and it is a technique, which is related to LA-ICP-MS, even though sampling and plasma are not separated. This feature is the reason for both its advantages (simplicity, cost) and its disadvantages (quantification capabilities, robustness) in comparison with LA-ICP-MS. I like how both techniques are advancing over time and I think that they both have a lot of potential.

What do you like and dislike the most about your work?

I especially like that I can both spend time in the lab and at the computer. This makes the work much more interesting and less repetitive. I also enjoy the freedom I have in planning and designing the experiments and see myself as lucky, because I can directly access so many tools and services at ETH, from the mechanical workshop to the chemical warehouse. What I do not like so much here in Zurich is the weather, which is quite dark and gray all year long. In addition, this is sometimes reflected on the mood of people, who tend to be gloomy.

What do you expect to be doing in 5 years time?

This is a very tough question. I hope that I will be doing something related to analytical chemistry, or at least science and technology in general. I am very open to new challenges, but I believe that I have learnt a lot about what is achievable nowadays with modern instrumentation and I would like to exploit this knowledge. I actually have a personal interest in forensics and criminology, which I may try to cultivate professionally.

What do you enjoy doing when you are not in the lab?

Contrarily to most Swiss people, I am not a very sporty person. I like to play tennis from time to time and to ski during the winter, but my principal hobbies are actually indoors. I play the piano – mostly jazz and blues – and I enjoy composing music on my computer. I have a digital piano, a synthesizer and I am a proud owner of a keytar, which is a keyboard that one can hold like a guitar. I also like digital photography and electronics, and to relax I like to watch movies and to play computer games.

Thanks a lot for your detailed answers, Luca!

Have a look at the most recents articles authored by Luca below!

Luca Flamigni, Joachim Koch, Helmar Wiltsche, Robert Brogioli, Sabrina Gschwind and Detlef Günther
J. Anal. At. Spectrom., 2012,27, 619-625
DOI: 10.1039/C2JA10317F, Paper
Sabrina Gschwind, Luca Flamigni, Joachim Koch, Olga Borovinskaya, Sebastian Groh, Kay Niemax and Detlef Günther
J. Anal. At. Spectrom., 2011,26, 1166-1174
DOI: 10.1039/C0JA00249F, Communication
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Allan Ure Bursary – Call for Applications

Allan Ure Bursary – Call for Applications
DEADLINE: 31st May 2013

The Allan Ure Bursary is awarded on an annual basis, alternately by the Atomic Spectroscopy Group of the Analytical Division of the Royal Society of Chemistry (ASG, AD, RSC) and the Atomic Spectrometry Updates (ASU) Editorial Board.

The award is presented to a scientist, at the start of their career, who the adjudicators believe has made a significant contribution to knowledge in the area of the application of atomic spectrometry to environmental science. The successful applicant will receive £500 to help with any expenses that may be of benefit to their career.

Who can apply?
Applicants need not be specialised analytical chemists and may come from fields as diverse as geology, biology, oceanography, geography and environmental science. They will, however, have to demonstrate that they use atomic spectrometry on a regular basis for their work. The scope of the Atomic Spectrometry Update – Environmental Analysis, published each year in the February issue of the Journal of Analytical Atomic Spectrometry may be taken as guidance.

Applications
Applications should be made electronically and consist of the applicant’s Curriculum Vitae plus a covering letter which clearly states how the bursary will be used and how the applicant believes this will benefit their career. The name of one referee (normally the applicant’s line manager) who is familiar with the applicant’s recent work should also be provided.

Applications may be submitted to ASG electronically to Dr A Fisher, afisher@plymouth.ac.uk

Further Information
Details of past winners and further information can be found on the ASG Website.

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Mars: Where the Sky is Orange

Sirven et al. featured on the front cover of JAAS, 2007, Issue 12

Yesterday the Royal Society of Chemistry had the pleasure to meet the driver of the Mars Curiosity rover Paolo Bellutta who revealed the secrets of Mars one year after the first ‘landing’ in 2012.

You might remember the paper published in 2007 in JAAS about ChemCam, the powerful instrument now functional part of the Mars Science Laboratory Curiosity rover used to study the red planet.

ChemCam uses laser induced breakdown spectroscopy (LIBS) to remotely analyse the surface of Mars looking into the chemistry of its rocks.

Jean-Baptiste Servien and colleagues at CEA Saclay, France, introduced the three chemometric approaches used by ChemCam to study the rocks on the surface of Mars in the paper entitled Feasibility study of rock identification at the surface of Marsby remote laser-induced breakdown spectroscopy and three chemometric methods.

Mars Curiosity rover on the red planet

Last August, Curiosity successfully landed at Gale Crater on the planet Mars. Paolo Bellutta, Rover’s driver from NASA’s Jet Propulsion Laboratory, explained what is behind a one-ton vehicle that is able to land in such a hostile place where the wind runs at 400Km/h, the temperature reaches -90°C and the sky turns orange.

How do we drive on Mars? And what are we doing on Mars ? To know everything about the Mars Mission watch the video soon available on The Reaction website.

Free for you until May 13th: Feasibility study of rock identification at the surface of Mars by remote laser-induced breakdown spectroscopy and three chemometric methods
Jean-Baptiste Sirven, Béatrice Sallé, Patrick Mauchien, Jean-Luc Lacour, Sylvestre Maurice and Gérard Manhès
J. Anal. At. Spectrom., 2007, 22, 1471-1480
DOI: 10.1039/B704868H

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Reconstructing how the Romans made glass

Man has been making glass since the third millennium BC and during the manufacture of ancient glass, antimony, in a metal or mineral form, was added to make it colourless or opaque.

Different antimony ores have slightly different antimony isotope ratios and researchers in Belgium and the UK have developed an inductively-coupled plasma mass spectrometry (ICP-MS) method to detect and quantify these tiny differences. By analysing samples of Roman glass, the team hope to uncover clues about how the glass was made and the geographical provenance of the raw materials.

 

To read the full article please visit Chemistry World.

Isotopic analysis of antimony using multi-collector ICP-mass spectrometry for provenance determination of Roman glass
Lara Lobo,Patrick Degryse,Andrew Shortland and Frank Vanhaecke
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA50018G

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Broad bobbin collar too fashionable?

While X-ray fluorescence (XRF) spectroscopy is a well-established technique for the investigation of paintings, the apparatus used are usually custom built and not widely available. Now, Matthias Alfeld and colleagues have developed a portable macro XRF spectrometer to look at paintings in situ.

The team used the device to look at a portrait by Govert Flinck, a Dutch painter who was a protégé of the great Rembrandt. Interestingly, they found that originally the subject was painted wearing a broad bobbin lace collar and long lace cuffs but this was toned down for the final version, possibly because it was too trendy.

Govert Flinck, Portrait of Dirck Jacobsz. Leeuw and elemental distribution images of the painting.

 To read the full article please visit Chemistry World.

A mobile instrument for in situ scanning macro-XRF investigation of historical paintings
Matthias Alfeld ,  Joana Vaz Pedroso, Margriet van Eikema Hommes, Geert Van der Snickt, Gwen Tauber, Jorik Blaas, Michael Haschke, Klaus Erler, Joris Dik and Koen Janssens
J. Anal. At. Spectrom., 2013, Advance Article
DOI: 10.1039/C3JA30341A

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Elemental Imaging Themed Issue: submissions still open

Soon we will be publishing a themed issue on Elemental Imaging in the field of analytical atomic spectrometry. The aim is to highlight imaging techniques and methods, including a mixture of both fundamental advances and exciting new applications.

Guest edited by:
Jorge Pisonero, University of Oviedo
Vincent Smentkowski, General Electric Global Research
Nerea Bordel, University of Oviedo

The submission deadline for the forthcoming themed issue of JAAS on Elemental Imaging was February 8th. We are still currently accepting submissions for this issue.

If you work in the field of elemental imaging submit your work today!

All articles will be peer-reviewed, and to be suitable for publication, must meet the usual quality and significance standards of the journal.  Please indicate in your covering letter that your article is to be considered for the Elemental Imaging theme. Email jaas-rsc@rsc.org for more information.

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Call for nominations YAS 2014 open now!

Journal of Analytical Atomic Spectrometry, 2010, Issue 3

YAS Cover 2010

We are pleased to announce the Call for nominations for the upcoming Young Analytical Scientists (YAS) themed issue of JAAS.

YAS is a special issue devoted to publishing the work of outstanding young analytical scientists within five years of their first academic or industrial appointment, working  in the area of atomic spectrometry and highlighting potentially high-impact research.

To know more about YAS 2014 please email us on JAAS-RSC@rsc.org.

Call for nominations are open until January 7th, 2013. Successful nominations will hear from the Guest Editor and Editorial Office the second week of January.

To view the last YAS issue, visit our website.

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2013 Bunsen-Kirchhoff Award for Analytical Spectroscopy

Deutscher Arbeitskreis für Angewandte Spektroskopie (DASp)Nominations are open for the 2013 “Bunsen-Kirchhoff-Preis für analytische Spektroskopie”. This award, from the German Working group for Applied Spectroscopy (DASp), honours the work of young scientists from universities, research institutes or industry who have made excellent contributions to analytical spectroscopy.

The Award consists of an award-document and an amount of €2500 sponsored by Perkin Elmer, and nominations are preferred for work in new and emerging areas, such as spectroscopy in nano compartments, and spectroscopy of biomolecules.

Each nomination should include:
 – a letter detailing the candidate’s accomplishments
 – a list of publications or recent work
 – scientific curriculum vitae stating the age of the candidate, their address and contact details

Nominations should be from a member of DASp but eligibility is open for any scientist meeting the requirements. Self-nomination is excluded. The recipient will be decided by a jury comprising current members of the board of DASp. Further information is available here.

The deadline for nominations is 15 December 2012, and all documents should be sent to:
Prof. Dr. Detlef Günther, President of the Jury for the Bunsen-Kirchhoff Award 2013
ETH Zürich, Laboratorium für Anorganische Chemie, Wolfgang-pauli-Str. 10, HCI G113, CH-8093 Zürich (Schweiz) detlef.guenther@inorg.chem.ethz.ch

Take a look at some recent papers from previous winners of the Bunsen-Kirchhoff Award:

2010 Janina Kneipp
Iodine as an elemental marker for imaging of single cells and tissue sections by laser ablation inductively coupled plasma mass spectrometry
Charlotte Giesen, Larissa Waentig, Thomas Mairinger, Daniela Drescher, Janina Kneipp, Peter H. Roos, Ulrich Panne and Norbert Jakubowski
J. Anal. At. Spectrom., 2011,26, 2160-2165
DOI: 10.1039/C1JA10227C

2009 Joachim Koch
Visualization, velocimetry, and mass spectrometric analysis of engineered and laser-produced particles passing through inductively coupled plasma sources
Luca Flamigni, Joachim Koch, Helmar Wiltsche, Robert Brogioli, Sabrina Gschwind and Detlef Günther
J. Anal. At. Spectrom., 2012,27, 619-625
DOI: 10.1039/C2JA10317F

2007 Jörg Bettmer
Analysis of hepcidin, a key peptide for Fe homeostasis, via sulfur detection by capillary liquid chromatography-inductively coupled plasma mass spectrometry
T. Konz, M. Montes-Bayón, J. Bettmer and A. Sanz-Medel
J. Anal. At. Spectrom., 2011,26, 334-340
DOI: 10.1039/C0JA00053A

Follow JAAS News on Twitter: @jaasnews

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