Archive for June, 2012

Archaeometry in JAAS

JAAS 2012, Archaeometry themed issue, front cover

Fan et al, J. Anal. At. Spectrom., 2012, 27, 821-826

In a recent issue of JAAS we highlighted work from around the world in the field of archaeometry. Also known as archaeological science, it is the use of scientific techniques to analyze archaeological materials, such as bone, ceramics, glass, and bronze.

The themed issue was guest edited by Patrick Degryse, from the University of Leuven (KU Leuven), Leuven, Belgium and the issue contained some exciting papers on topics including Roman glass, human teeth, medieval village populations, and metallurgy in China. Click through here to take a look at the issue or read about it in the blog. The below papers will be free to access for 2 weeks.

Some HOT papers from this themed issue include;

Roman glass across the Empire: an elemental and isotopic characterization
Monica Ganio, Sara Boyen, Thomas Fenn, Rebecca Scott, Sofie Vanhoutte, Domingo Gimeno and Patrick Degryse
J. Anal. At. Spectrom., 2012, 27, 743-753
DOI: 10.1039/C2JA10355A

A summary of strontium and oxygen isotope variation in archaeological human tooth enamel excavated from Britain
J. A. Evans, C. A. Chenery and J. Montgomery
J. Anal. At. Spectrom., 2012, 27, 754-764
DOI: 10.1039/C2JA10362A

Here in JAAS we have published many papers on the topic of archaeometry in the past. Take a look at a few selected papers listed below. If you have a paper you are looking to publish in this field, why not try submitting to JAAS.

Open ablation cell for LA-ICP-MS investigations of historic objects
Barbara Wagner and Wojciech Jędral
J. Anal. At. Spectrom., 2011, 26, 2058-2063
DOI: 10.1039/C1JA10137D

Micro and Surface Analysis in Art and Archaeology
F. Adams, A. Adriaens, A. Aerts, I. De Raedt, K. Janssens and O. Schalm
J. Anal. At. Spectrom., 1997, 12, 257-265
DOI: 10.1039/A606091I

Application of laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS) for the investigation of ancient silver coins
Guillaume Sarah, Bernard Gratuze and Jean-Noël Barrandon
J. Anal. At. Spectrom., 2007, 22, 1163-1167
DOI: 10.1039/B704879C

Evaluation of different calibration methods in inductively coupled plasma atomic emission spectrometric analysis of certified glass materials and archaeological glass specimens
G. A. Zachariadis, A. N. Anthemidis and J. A. Stratis
J. Anal. At. Spectrom., 2003, 18, 358-366
DOI: 10.1039/B301098H

Synchrotron radiation and cultural heritage: combined XANES/XRF study at Mn K-edge of blue, grey or black coloured palaeontological and archaeological bone material
Ina Reiche and Emilie Chalmin
J. Anal. At. Spectrom., 2008, 23, 799-806
DOI: 10.1039/B717442J

A study on gold and copper provenance for Romanian prehistoric objects using micro-SR XRF
Bogdan Constantinescu, Angela Vasilescu, Martin Radtke and Uwe Reinholz
J. Anal. At. Spectrom., 2011, 26, 917-921
DOI: 10.1039/C0JA00215A

Synchrotron radiation and laboratory micro X-ray computed tomography—useful tools for the material identification of prehistoric objects made of ivory, bone or antler
I. Reiche, K. Müller, A. Staude, J. Goebbels and H. Riesemeier
J. Anal. At. Spectrom., 2011, 26, 1802-1812
DOI: 10.1039/C0JA00246A

Quantitative characterisation of the leaching of lead and other elements from glazed surfaces of historical ceramics
I. Szalóki, M. Braun and R. Van Grieken
J. Anal. At. Spectrom., 2000, 15, 843-850
DOI: 10.1039/B000746N

Integrated X-ray and neutron-based analysis of bronze artefacts from the Ligurian settlement of Guardamonte-Monte Vallassa
Roberta Cattaneo, Cristina Chiaramonte Trerè, Lucia Mordeglia, Giuseppe Gorini, Enrico Perelli Cippo, Laura Bartoli, Winfried Kockelmann and Antonella Scherillo
J. Anal. At. Spectrom., 2011, 26, 1024-1029
DOI: 10.1039/C0JA00259C

Development of a new method for Pb isotopic analysis of archaeological artefacts using single-collector ICP-dynamic reaction cell-MS
David De Muynck, Christophe Cloquet and Frank Vanhaecke
J. Anal. At. Spectrom., 2008, 23, 62-71
DOI: 10.1039/B709461B

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HOT Article: Evaluating silicagels for Pb isotopic analysis

The analysis of Pb isotopes is used in several fields, including ore formation studies, environmental studies and U–Pb geochronology. But sample sizes can also be very small, making precise measurements difficult. One method to compensate for this, is adding silicagel as an ionisation activator for Pb isotopic analysis. Magdalena H. Huyskens, Tsuyoshi Iizuka and Yuri Amelin at The Australian National University, Canberra, Australia, have run a series of tests, comparing three commercially available colloidal silicagels. Read their results by clicking on the title below.

Huyskens et al., J. Anal. At. Spectrom., 2012, Advance Article

Evaluation of colloidal silicagels for lead isotopic measurements using thermal ionisation mass spectrometry
Magdalena H. Huyskens,  Tsuyoshi Iizuka and Yuri Amelin
J. Anal. At. Spectrom., 2012, Advance Article
DOI: 10.1039/C2JA30083D

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50-jarig jubileum in Tilburg

A symposium celebrating 50-years of Atomic Spectroscopy in The Netherlands was held on June 7 2012 in Tilburg (The Netherlands). The conference was organized by the Atomic Spectroscopy Working Group (WAS), chaired by JAAS Advisory board member Prof. Margaretha de Loos-Vollebregt, following the success of previous events (e.g., 40 and 45-year celebrations). 130 attendees from the academia and the industry gathered in the nice venue selected for the occasion (Villa de Vier Jaargetijden in Tilburg), where the Invited Speakers Jean-Michel Mermet, Martín Resano, Leo de Galan, Jochen Vogl, Michael Sperling, Ralph Sturgeon and Joris Dik presented their latest work. You can find some recent examples of these authors’ work below.

Great to see that Atomic Spectroscopy is still in very good shape in The Netherlands!

Invited speakers sharing dinner in Tilburg

Universal calibration for metal determination in fuels and biofuels by inductively coupled plasma atomic emission spectrometry based on segmented flow injection and a 350 °C heated chamber

Raquel Sánchez, José Luis Todolí, Charles-Philippe Lienemann and Jean-Michel Mermet, J. Anal. At. Spectrom., 2012,27, 937-945

Direct determination of sulfur in solid samples by means of high-resolution continuum source graphite furnace molecular absorption spectrometry using palladium nanoparticles as chemical modifier

Martín Resano and María R. Flórez, J. Anal. At. Spectrom., 2012,27, 401-412

Development and validation of a single collector SF-ICPMS procedure for the determination of boron isotope ratios in water and food samples

Jochen Vogl, Martin Rosner and Wolfgang Pritzkow, J. Anal. At. Spectrom., 2011,26, 861-869

Speciation analysis of the antirheumatic agent Auranofin and its thiol adducts by LC/ESI-MS and LC/ICP-MS

Anastasia Albert, Christine Brauckmann, Franziska Blaske, Michael Sperling, Carsten Engelhard and Uwe Karst, J. Anal. At. Spectrom., 2012,27, 975-981

Some speculations on the mechanisms of photochemical vapor generation

Ralph E. Sturgeon and Patricia Grinberg, J. Anal. At. Spectrom., 2012,27, 222-231

Optimization of mobile scanning macro-XRF systems for the in situ investigation of historical paintings

Matthias Alfeld, Koen Janssens, Joris Dik, Wout de Nolf and Geert van der Snickt, J. Anal. At. Spectrom., 2011,26, 899-909

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5 papers to read before you cite

Everybody love lists and I have been told than JAAS readers are no different. Thus, I decided to make a very short list of recent JAAS papers I enjoyed, just for the sake of discussion. In no particular order, here are five 2012 JAAS papers I recently read and liked:

1. Considerations for measurement of individual nanoparticles or microparticles by ICP-MS: determination of the number of particles and the analyte mass in each particle

John W. Olesik and Patrick J. Gray, J. Anal. At. Spectrom., 2012,27, 1143-1155

2. Graphite tubes with small internal diameters tailored for high-resolution continuum source graphite furnace atomic absorption spectrometry

Mao Dong Huang, Helmut Becker-Ross, Michael Okruss, Sebastian Geisler and Stefan Florek, J. Anal. At. Spectrom., 2012, 27, 982-988

3. Depth dependent element ratios in fluid inclusion analysis by laser ablation ICP-MS

Marcel Guillong and Thomas Pettke, J. Anal. At. Spectrom., 2012, 27, 505-508

4. Pulsed glow discharge time of flight mass spectrometry for the screening of polymer-based coatings containing brominated flame retardants

Claudia González de Vega, Lara Lobo, Beatriz Fernández, Nerea Bordel, Rosario Pereiro and Alfredo Sanz-Medel, J. Anal. At. Spectrom., 2012, 27, 318-326

5. Improving acquisition times of elemental bio-imaging for quadrupole-based LA-ICP-MS

Jessica Lear, Dominc Hare, Paul Adlard, David Finkelstein and Philip Doble, J. Anal. At. Spectrom., 2012, 27, 159-164

And you? Which papers did you particularly like? Please let us know!

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Issue 7 online: themed issue on Nanoanalysis

JAAS, 2012, Issue 7, front cover

Front cover: Nischwitz & Goenaga-Infante, J. Anal. At. Spectrom., 2012, 27, 1084-1092

The latest issue of JAAS is now online, which is a themed issue on Nanoanalysis. Guest Edited by Petra Krystek, Zoltán Mester and Kay Niemax, this themed issue highlights an important area of atomic spectrometry. May Copsey and I introduce the issue on behalf of the Guest Editors in an Editorial:

A snapshot of atomic and elemental analysis on the nanoscale
May Copsey and Vibhuti Patel
J. Anal. At. Spectrom., 2012, 27, 1049-1049
DOI: 10.1039/C2JA90038F

The front cover features a paper from Volker Nischwitz and Heidi Goenaga-Infante, which presents the first systematic comparison and optimisation of extraction methods for the characterisation of titanium dioxide nanoparticles in sunscreens using FFF-ICP-MS.

Improved sample preparation and quality control for the characterisation of titanium dioxide nanoparticles in sunscreens using flow field flow fractionation on-line with inductively coupled plasma mass spectrometry
Volker Nischwitz and Heidi Goenaga-Infante
J. Anal. At. Spectrom., 2012, 27, 1084-1092
DOI: 10.1039/C2JA10387G

JAAS, 2012, Issue 7, inside front cover

Franze et al., J. Anal. At. Spectrom., 2012, 27, 1074-1083

The inside front cover highlights a paper from JAAS News contributor Carsten Engelhard and colleagues. They compare the analytical performance of three sample introduction systems for the characterization of 20–100 nm Ag nanoparticles.

Single particle inductively coupled plasma mass spectrometry: evaluation of three different pneumatic and piezo-based sample introduction systems for the characterization of silver nanoparticles
Bastian Franze, Ingo Strenge and Carsten Engelhard
J. Anal. At. Spectrom., 2012, 27, 1074-1083
DOI: 10.1039/C2JA00003B

Other HOT articles in this issue are:

Critical Review: SIMS imaging of the nanoworld: applications in science and technology
Mathias Senoner and Wolfgang E. S. Unger
J. Anal. At. Spectrom., 2012, 27, 1050-1068
DOI: 10.1039/C2JA30015J

Laser-induced breakdown spectroscopy for analysis of micro and nanoparticles
Prasoon K. Diwakar, Kristofer H. Loper, Anna-Maria Matiaske and David. W. Hahn
J. Anal. At. Spectrom., 2012, 27, 1110-1119
DOI: 10.1039/C2JA30012E

Considerations for measurement of individual nanoparticles or microparticles by ICP-MS: determination of the number of particles and the analyte mass in each particle
John W. Olesik and Patrick J. Gray
J. Anal. At. Spectrom., 2012, 27, 1143-1155
DOI: 10.1039/C2JA30073G

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Top Ten most-read JAAS articles in April

This month sees the following articles in JAAS that are in the top ten most accessed in April:

Single particle inductively coupled plasma mass spectrometry: evaluation of three different pneumatic and piezo-based sample introduction systems for the characterization of silver nanoparticles 
Bastian Franze, Ingo Strenge and Carsten Engelhard  
J. Anal. At. Spectrom., 2012, Advance Article 
DOI: 10.1039/C2JA00003B  

Overcoming challenges in analysis of polydisperse metal-containing nanoparticles by single particle inductively coupled plasma mass spectrometry 
Robert B. Reed, Christopher P. Higgins, Paul Westerhoff, Soheyl Tadjiki and James F. Ranville 
J. Anal. At. Spectrom., 2012, Advance Article 
DOI: 10.1039/C2JA30061C  

Atomic spectrometry update. Clinical and biological materials, foods and beverages 
Andrew Taylor, Martin P. Day, John Marshall, Marina Patriarca and Mark White  
J. Anal. At. Spectrom., 2012, 27, 537-576 
DOI: 10.1039/C2JA90005J   

Comparison of novel and conventional calibration techniques for the analysis of urine samples using plasma source mass spectrometry combined with a new dual-drop-on-demand aerosol generator 
Jan O. Orlandini v. Niessen, Jan H. Petersen, J. Niklas Schaper and Nicolas H. Bings  
J. Anal. At. Spectrom., 2012, Advance Article 
DOI: 10.1039/C2JA30039G  

A summary of strontium and oxygen isotope variation in archaeological human tooth enamel excavated from Britain 
J. A. Evans, C. A. Chenery and J. Montgomery  
J. Anal. At. Spectrom., 2012, 27, 754-764 
DOI: 10.1039/C2JA10362A  

Improved sample preparation and quality control for the characterisation of titanium dioxide nanoparticles in sunscreens using flow field flow fractionation on-line with inductively coupled plasma mass spectrometry 
Volker Nischwitz and Heidi Goenaga-Infante  
J. Anal. At. Spectrom., 2012, Advance Article 
DOI: 10.1039/C2JA10387G  

The four players in the Analytical Performance 
L. de Galan  
J. Anal. At. Spectrom., 2012, Advance Article 
DOI: 10.1039/C2JA90011D  

Strontium and lead isotope ratios in human hair: investigating a potential tool for determining recent human geographical movements 
Laura Font, Gerard van der Peijl, Isis van Wetten, Pieter Vroon, Bas van der Wagt and Gareth Davies  
J. Anal. At. Spectrom., 2012, 27, 719-732 
DOI: 10.1039/C2JA10361C  

Atomic spectrometry update. Environmental analysis 
Owen T. Butler, Warren R. L. Cairns, Jennifer M. Cook and Christine M. Davidson  
J. Anal. At. Spectrom., 2012, 27, 187-221 
DOI: 10.1039/C1JA90057A  

Atomic spectrometry update. Industrial analysis: metals, chemicals and advanced materials
 
Simon Carter, Andy S. Fisher, Phill S. Goodall, Michael W. Hinds, Steve Lancaster and Sian Shore  
J. Anal. At. Spectrom., 2011, 26, 2319-2372 
DOI: 10.1039/C1JA90047A 

Why not take a look at the articles today and blog your thoughts and comments below.

Fancy submitting an article to JAAS?  Then why not submit to us today!

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HOT Article: Measuring individual particles

Olesik & Gray, J. Anal. At. Spectrom., 2012, Advance Article

This month we have a HOT article from our Associate Editor for the Americas, John W. Olesik and Patrick J. Gray, from Ohio State University, USA. Nanoparticles and microparticles are used in so many products nowadays, but the rapid, simultaneous characterization of their elemental chemical composition is very tricky. In the following paper, the unique considerations to determine the number of particles per liter and analyte mass (particle size) distributions from single particle ICP-MS measurements using quadrupole or sequential sector field mass spectrometry is explored.

Considerations for measurement of individual nanoparticles or microparticles by ICP-MS: determination of the number of particles and the analyte mass in each particle
John W. Olesik and Patrick J. Gray
J. Anal. At. Spectrom., 2012, Advance Article
DOI: 10.1039/C2JA30073G

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