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Analytical methods for forensic science

Forensic kitBy definition, forensic science is the use of science to answer questions that are of interest to a legal system. Today the average person is far more familiar with forensics thanks to popular televisions series, books and films where the pivotal clue is usually discovered by the scientist. Forensic science has also been in the headlines a lot lately in the UK with the recent closure of the Forensic Science Service.

Specialties in forensics can include the analysis of blood, DNA, drugs, arson residues, documents, fibres, hair and explosives, just to name a few.

Analytical Methods presents an excellent forum for such work, and below is a sample of the high-quality work we have published in this area.  These articles are free to access until the 30th May 2012 so make the most of this and take a look!

Development and validation of an analytical method for hydrocarbon residues using gas chromatography-mass spectrometry
Aree Choodum and Niamh Nic Daeid
Anal. Methods, 2011, 3, 1136-1142, DOI: 10.1039/C0AY00702A

A method based on time domain nuclear magnetic resonance for the forensic differentiation of latex gloves
Michele Mauri, Lucio Mauri, Valerio Causin and Roberto Simonutti
Anal. Methods, 2011, 3, 1802-1809, DOI: 10.1039/C1AY05131H

Crime scene investigation III: Exploring the effects of drugs of abuse and neurotransmitters on Bloodstain Pattern Analysis
Bethany A. J. Larkin, Meerna El-Sayed, Dale A. C. Brownson and Craig E. Banks
Anal. Methods, 2012, 4, 721-729, DOI: 10.1039/C2AY05762J

Comparison of extraction methods for the removal of volatile organic compounds (VOCs) present in sorbents used for human scent evidence collection
Paola A. Prada, Allison M. Curran and Kenneth G. Furton
Anal. Methods, 2010, 2, 470-478, DOI: 10.1039/B9AY00239A

Separation and identification of anions using porous graphitic carbon and electrospray ionization mass spectrometry: Application to inorganic explosives and their post blast residues
Josh Cummins, Jason Hull, Kelley Kitts and John V. Goodpaster
Anal. Methods, 2011, 3, 1682-1687, DOI: 10.1039/C1AY05143A

Handprint with chemical structure behindDetermination of some banned aromatic amines in waste water using micellar liquid chromatography
Sandeep-Kumar Mourya, Devasish Bose, Abhilasha Durgbanshi, Josep Esteve-Romero and Samuel Carda-Broch
Anal. Methods, 2011, 3, 2032-2040, DOI: 10.1039/C0AY00602E

Identification of fluid and substrate chemistry based on automatic pattern recognition of stains
Namwon Kim, Zhenguo Li, Cedric Hurth, Frederic Zenhausern, Shih-Fu Chang and Daniel Attinger
Anal. Methods, 2012, 4, 50-57, DOI: 10.1039/C1AY05338H

Optimization of micellar LC conditions for separation of opium alkaloids and their determination in pharmaceutical preparations
Artem U. Kulikov, Alexander P. Boichenko and Aleksey G. Verushkin
Anal. Methods, 2011, 3, 2749-2757, DOI: 10.1039/C1AY05389B

Multivariate analyses of UV-Vis absorption spectral data from cachaça wood extracts: a model to classify aged Brazilian cachaças according to the wood species used
Alexandre Ataide da Silva, Denis De Keukeleire, Daniel Rodrigues Cardoso and Douglas Wagner Franco
Anal. Methods, 2012, 4, 642-646, DOI: 10.1039/C2AY05670D

Laser induced breakdown spectroscopy for rapid identification of different types of paper for forensic application
Arnab Sarkar, Suresh K. Aggarwal and D. Alamelu
Anal. Methods, 2010, 2, 32-36, DOI: 10.1039/B9AY00145J

Polymers on the crime scene: How can analytical chemistry help to exploit the information from these mute witnesses?
Valerio Causin
Anal. Methods, 2010, 2, 792-804, DOI: 10.1039/C0AY00115E

Crime scene investigation: The effect of drug contaminated bloodstains on bloodstain pattern analysis
Dale A. C. Brownson and Craig E. Banks
Anal. Methods, 2010, 2, 1885-1889, DOI: 10.1039/C0AY00537A

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Developments and applications of electrophoresis

Electrophoresis is a very useful separation method employed in a great variety of applications, including the separation and analysis of biological samples (e.g. DNA and proteins) and environmental samples (e.g. pesticide or pollutant analysis).  Electrophoresis comes in various different forms (capillary or gel electrophoresis for example) making it a very versatile and adaptable technique.

Analytical Methods presents an excellent forum for advances and applications of this technique, and below is a sample of the high-quality work we have published in this area.  These articles are free to access until the 13th February 2012 so make the most of this and take a look!

And don’t forget to stay informed of all our latest content by signing up to our e-alert or following us on Twitter: @methodsrsc and @analystrsc.

EndoV/DNA ligase mutation scanning assay using microchip capillary electrophoresis and dual-color laser-induced fluorescence detection, Akira Kotani, Małgorzata A. Witek, John K. Osiri, Hong Wang, Rondedrick Sinville, Hanna Pincas, Francis Barany and Steven A. Soper, Anal. Methods, 2012, 4, 58-64

Thermally responsive polymer as a sieving matrix of proteins in capillary gel electrophoresis, Chun Yang, Chunyan Chang, Jun Wang, Qishu Qu, Xiaoya Hu and Yang Wang, Anal. Methods, 2011, 3, 2717-2720

Assay design considerations for use of affinity aptamer amplification in ultra-sensitive protein assays using capillary electrophoresis, Kris P. F. Janssen, Karel Knez, Jeroen Pollet, Scott J. Roberts, Jan Schrooten and Jeroen Lammertyn, Anal. Methods, 2011, 3, 2156-2159

Recent advances of enantioseparations in capillary electrophoresis and capillary electrochromatography, Huang Lu and Guonan Chen, Anal. Methods, 2011, 3, 488-508

Rapid speciation analysis of mercury by short column capillary electrophoresis on-line coupled with inductively coupled plasma mass spectrometry, Bao-Hui Li, Anal. Methods, 2011, 3, 116-121

Rapid prototyping of polymeric electrophoresis microchips with integrated copper electrodes for contactless conductivity detection, Wendell Karlos Tomazelli Coltro, José Alberto Fracassi da Silva and Emanuel Carrilho, Anal. Methods, 2011, 3, 168-172

Speciation of organotin compounds in environmental samples with semi-permanent coated capillaries by capillary electrophoresis coupled with inductively coupled plasma mass spectrometry, Jing Sun, Bin He, Yongguang Yin, Lu Li and Guibin Jiang, Anal. Methods, 2010, 2, 2025-2031

Determination of paraquat and diquat preconcentrated with N doped TiO2nanotubes solid phase extraction cartridge prior to capillary electrophoresis, Qingxiang Zhou, Jinli Mao, Junping Xiao and Guohong Xie, Anal. Methods, 2010, 2, 1063-1068

Ionic liquids in the assay of proteins, Xuwei Chen, Jiawei Liu and Jianhua Wang, Anal. Methods, 2010, 2, 1222-1226

Ionic mobility of the solvated proton and acid–base titration in a four-compartment capillary electrophoresis system, Renata Mayumi Saito, José Geraldo Alves Brito-Neto, Fernando Silva Lopes, Lucas Blanes, Eric Tavares da Costa, Denis Tadeu Rajh Vidal, Guilherme Minoru Hotta and Claudimir Lucio do Lago, Anal. Methods, 2010, 2, 164-170

Application of dispersive liquid–liquid microextraction combined with sweeping micellar electrokinetic chromatography for trace analysis of six carbamate pesticides in apples, Shuaihua Zhang, Chao Li, Shuangju Song, Tao Feng, Chun Wang and Zhi Wang, Anal. Methods, 2010, 2, 54-62

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Analytical methods for food and agriculture

Images courtesy of Fotolia (left) and iStock (right)

Analysis of food and agricultural products or materials is a very topical subject at present.  Development of sensitive, accurate and versatile analytical methods are important in order to monitor food and agricultural standards, understand the composition or structure of food, and to detect levels of toxic or unwanted chemicals.  Recent examples include monitoring levels of melamine in milk or pesticide residues in food.

Analytical Methods presents an excellent forum for such work, and below is a sample of the high-quality work we have published in this area.  These articles are free to access until the 13th January 2012 so make the most of this and take a look!

And don’t forget to stay informed of all our latest content by signing up to our e-alert or following us on Twitter: @methodsrsc and @analystrsc

Solid phase extraction and sequential elution for pre-concentration of traces of Mn and Zn in analysis of honey by flame atomic absorption spectrometry, Pawel Pohl, Helena Stecka and Piotr Jamroz, Anal. Methods, 2012, DOI: 10.1039/C1AY05637A

A simple and high-throughput method of ultrasonic extraction-capillary electrophoresis for determination of melamine in milk, Yun-Kai Lv, Yue-Na Sun, Li-Min Wang, Cui-Ling Jia and Han-Wen Sun, Anal. Methods, 2011, 3, 2557-2561

Methods of sample preparation for determination of veterinary residues in food matrices by porous monolith microextraction-based techniques, Fang Wei and Yu-Qi Feng, Anal. Methods, 2011, 3, 1246-1256

Electroanalytical determination of carbendazim by square wave adsorptive stripping voltammetry with a multiwalled carbon nanotubes modified electrode, Williame Farias Ribeiro, Thiago Matheus Guimarães Selva, Ilanna Campelo Lopes, Elaine Cristina S. Coelho, Sherlan Guimarães Lemos, Fabiane Caxico de Abreu, Valberes Bernardo do Nascimento and Mário César Ugulino de Araújo, Anal. Methods, 2011, 3, 1202-1206

Fluorescence images combined to statistic test for fingerprinting of citrus plants after bacterial infection, Fabíola Manhas Verbi Pereira, Débora Marcondes Bastos Pereira Milori, Edenir Rodrigues Pereira-Filho, André Leonardo Venâncio, Mariana de Sá Tavares Russo, Polyana Kelly Martins and Juliana Freitas-Astúa, Anal. Methods, 2011, 3, 552-556

Preconcentration and determination of pyrethroid insecticides in water with ionic liquid dispersive liquid-phase microextraction in combination with high performance liquid chromatography, Qingxiang Zhou, Xiaoguo Zhang and Guohong Xie, Anal. Methods, 2011, 3, 356-361

Rapid Raman mapping for chocolate analysis, I. A. Larmour, K. Faulds and D. Graham, Anal. Methods, 2010, 2, 1230-1232

A LC/UV/Vis method for determination of cyanocobalamin (VB12) in multivitamin dietary supplements with on-line sample clean-up, Pei Chen, Wayne R. Wolf, Isabel Castanheira and Ana Sanches-Silva, Anal. Methods, 2010, 2, 1171-1175

Simultaneous determination of paclobutrazol and myclobutanil enantiomers in water and soil using enantioselective reversed-phase liquid chromatography, Qin Tian, Zhiqiang Zhou, Chunguang Lv, Yi Huang and Liping Ren, Anal. Methods, 2010, 2, 617-622

Application of dispersive liquid–liquid microextraction combined with sweeping micellar electrokinetic chromatography for trace analysis of six carbamate pesticides in apples, Shuaihua Zhang, Chao Li, Shuangju Song, Tao Feng, Chun Wang and Zhi Wang, Anal. Methods, 2010, 2, 54-62

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